{"title":"pd催化的无co羰基化:2,4,6-三氯苯基3,4-二氢萘-2-羧酸盐的制备","authors":"H. Konishi","doi":"10.15227/ORGSYN.097.0125","DOIUrl":null,"url":null,"abstract":"Palladium-catalyzed carbonylation of organic (pseudo)halides has received much attention because of its versatility for the synthesis of carbonyl-containing compounds. This article discusses the preparation of 2,4,6-trichlorophenyl 3,4-dihydronaphthalene-2-carboxylate using Pd-catalyzed external-CO-free carbonylation. It also discusses the characterization data of 2,4,6-trichlorophenyl 3,4-dihydronaphthalene-2-carboxylate. Keywords: Pd-Catalysis; 2,4,6-Trichlorophenyl formate; 2,4,6-Trichlorophenyl 3,4-dihydronaphthalene-2-carboxylate; 3,4-Dihydronaphthalen-2-yl trifluoromethanesulfonate","PeriodicalId":19576,"journal":{"name":"Organic Syntheses","volume":"64 1","pages":"125-138"},"PeriodicalIF":0.7000,"publicationDate":"2020-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Pd-Catalyzed External-CO-Free Carbonylation: Preparation of 2,4,6-Trichlorophenyl 3,4- Dihydronaphthalene-2-Carboxylate\",\"authors\":\"H. Konishi\",\"doi\":\"10.15227/ORGSYN.097.0125\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Palladium-catalyzed carbonylation of organic (pseudo)halides has received much attention because of its versatility for the synthesis of carbonyl-containing compounds. This article discusses the preparation of 2,4,6-trichlorophenyl 3,4-dihydronaphthalene-2-carboxylate using Pd-catalyzed external-CO-free carbonylation. It also discusses the characterization data of 2,4,6-trichlorophenyl 3,4-dihydronaphthalene-2-carboxylate. Keywords: Pd-Catalysis; 2,4,6-Trichlorophenyl formate; 2,4,6-Trichlorophenyl 3,4-dihydronaphthalene-2-carboxylate; 3,4-Dihydronaphthalen-2-yl trifluoromethanesulfonate\",\"PeriodicalId\":19576,\"journal\":{\"name\":\"Organic Syntheses\",\"volume\":\"64 1\",\"pages\":\"125-138\"},\"PeriodicalIF\":0.7000,\"publicationDate\":\"2020-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Organic Syntheses\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.15227/ORGSYN.097.0125\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, ORGANIC\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Organic Syntheses","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.15227/ORGSYN.097.0125","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, ORGANIC","Score":null,"Total":0}
Pd-Catalyzed External-CO-Free Carbonylation: Preparation of 2,4,6-Trichlorophenyl 3,4- Dihydronaphthalene-2-Carboxylate
Palladium-catalyzed carbonylation of organic (pseudo)halides has received much attention because of its versatility for the synthesis of carbonyl-containing compounds. This article discusses the preparation of 2,4,6-trichlorophenyl 3,4-dihydronaphthalene-2-carboxylate using Pd-catalyzed external-CO-free carbonylation. It also discusses the characterization data of 2,4,6-trichlorophenyl 3,4-dihydronaphthalene-2-carboxylate. Keywords: Pd-Catalysis; 2,4,6-Trichlorophenyl formate; 2,4,6-Trichlorophenyl 3,4-dihydronaphthalene-2-carboxylate; 3,4-Dihydronaphthalen-2-yl trifluoromethanesulfonate
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