{"title":"用溶胶-凝胶法从蔗渣灰中合成Y型沸石并对其进行表征","authors":"S. Ali, S. Amalia, A. Fasya","doi":"10.18860/AL.V4I1.3069","DOIUrl":null,"url":null,"abstract":"Zeolite Synthesis Y is done using sol-gel method on the molar composition of 10Na 2 O: 15 SiO 2 : x Al 2 O 3 : 300 H 2 O with Si/Al on ratio of 2,43 and hydrothermal temperatures variations of 60, 80 and 100 °C. Characterization includes XRD to discover crystallinity and the purity of zeolite, FTIR for the analysis of functional groups and of the surface width with the adsorption of methylene blue. XRD result shows that the formed zeolites Y is still mixed with zeolite P, the best result in synthesis with hydrothermal temperatures of 80 °C. FTIR analysis showsthat all zeolite synthesis contain a common functionO-Si-O/O-Al-O and double ring. The surface area of zeolite Y at 60, 80 and 100 °C is 22,5522; 23,0603 and22,9898m 2 /gram. Keywords : Bagasse, sol-gel, temperature hydrothermal, zeolite Y","PeriodicalId":31035,"journal":{"name":"Alchemy Journal of Chemistry","volume":"4 1","pages":"88-92"},"PeriodicalIF":0.0000,"publicationDate":"2015-12-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Synthesis and Characterization of Zeolite Y From Bagasse Ash with Hydrothermal Temperatures Variations Using The Sol-Gel Method\",\"authors\":\"S. Ali, S. Amalia, A. Fasya\",\"doi\":\"10.18860/AL.V4I1.3069\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Zeolite Synthesis Y is done using sol-gel method on the molar composition of 10Na 2 O: 15 SiO 2 : x Al 2 O 3 : 300 H 2 O with Si/Al on ratio of 2,43 and hydrothermal temperatures variations of 60, 80 and 100 °C. Characterization includes XRD to discover crystallinity and the purity of zeolite, FTIR for the analysis of functional groups and of the surface width with the adsorption of methylene blue. XRD result shows that the formed zeolites Y is still mixed with zeolite P, the best result in synthesis with hydrothermal temperatures of 80 °C. FTIR analysis showsthat all zeolite synthesis contain a common functionO-Si-O/O-Al-O and double ring. The surface area of zeolite Y at 60, 80 and 100 °C is 22,5522; 23,0603 and22,9898m 2 /gram. Keywords : Bagasse, sol-gel, temperature hydrothermal, zeolite Y\",\"PeriodicalId\":31035,\"journal\":{\"name\":\"Alchemy Journal of Chemistry\",\"volume\":\"4 1\",\"pages\":\"88-92\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2015-12-02\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Alchemy Journal of Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.18860/AL.V4I1.3069\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Alchemy Journal of Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.18860/AL.V4I1.3069","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1
摘要
分子筛的摩尔组成为10Na 2o: 15 sio2: x Al 2o3: 300 h2o，硅铝比为2,43，水热温度分别为60、80和100℃，采用溶胶-凝胶法制备。表征包括XRD来发现沸石的结晶度和纯度，FTIR用于分析官能团和亚甲基蓝吸附后的表面宽度。XRD结果表明，形成的Y型沸石仍与P型沸石混合，在水热温度为80℃时合成效果最好。FTIR分析表明，所有合成的沸石都含有一个共同的功能- si - o /O-Al-O和双环。沸石Y在60、80、100℃时的比表面积分别为22、5522;23,0603和22,9898米2 /克。关键词:甘蔗渣，溶胶-凝胶，温度水热，Y型沸石
Synthesis and Characterization of Zeolite Y From Bagasse Ash with Hydrothermal Temperatures Variations Using The Sol-Gel Method
Zeolite Synthesis Y is done using sol-gel method on the molar composition of 10Na 2 O: 15 SiO 2 : x Al 2 O 3 : 300 H 2 O with Si/Al on ratio of 2,43 and hydrothermal temperatures variations of 60, 80 and 100 °C. Characterization includes XRD to discover crystallinity and the purity of zeolite, FTIR for the analysis of functional groups and of the surface width with the adsorption of methylene blue. XRD result shows that the formed zeolites Y is still mixed with zeolite P, the best result in synthesis with hydrothermal temperatures of 80 °C. FTIR analysis showsthat all zeolite synthesis contain a common functionO-Si-O/O-Al-O and double ring. The surface area of zeolite Y at 60, 80 and 100 °C is 22,5522; 23,0603 and22,9898m 2 /gram. Keywords : Bagasse, sol-gel, temperature hydrothermal, zeolite Y
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