含炭黑多孔陶瓷的初步研究

IF 1.4 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY AIMS Materials Science Pub Date : 2023-01-01 DOI:10.3934/matersci.2023041
Mohamed Lokman Jalaluddin, U. Azlan, Mohd Warikh Abd Rashid
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引用次数: 0

摘要

本文研究了在粘土(高岭石)、二氧化硅(二氧化硅)和长石的混合物中加入不同含量的炭黑(CB)制备多孔陶瓷。结果包括表观孔隙率、相对密度、微观结构和孔隙特性、抗折强度和相形成。经观察,1200℃的烧结温度是本工作的最佳烧结温度。与不含炭黑的样品相比,炭黑含量对陶瓷的表观孔隙率和相对密度有很大的影响。这可能是由于陶瓷断口表面的SEM图像中存在多孔结构。结果还表明,炭黑的加入使孔隙尺寸变小,孔隙分布更加均匀。扫描电镜观察到,多孔陶瓷中孔洞的形成主要是由于炭黑微球在高温下失去形状。由于炭黑的存在,烧结样品的抗折强度从60 MPa平均降低到55 MPa,这是众所周知的降低高孔隙率的机械性能的典型因素。在XRD结果中,白云母相由少数具有显著强度的峰代表,其余峰为未确定的相。最强的峰在2θ角26°处,表明钾和铝以硅酸盐矿物的形式存在。
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A preliminary study of porous ceramics with carbon black contents
This paper is a study of porous ceramics from a mixture of clay (kaolinite), silica (silicon dioxide), and feldspar by adding the carbon black (CB) with different contents. The results were presented in terms of apparent porosity, relative density, microstructure and porous characteristic, flexural strength and phase formation. As observed, the sintering at 1200 ℃ is the optimum temperature in this work. In comparison to the samples without CB content, the apparent porosity and relative density of ceramics are highly dependent on the CB contents. This might be attributed to the presence of porous structure as seen in SEM images on the fracture surface of ceramics. It also revealed that the addition of CB resulted in smaller pore sizes and a more uniform pore distribution. The creation of pores in porous ceramics was mainly attributed to the loss of shape of CB microspheres at high temperatures, as observed from SEM. The flexural strength of the sintered samples exhibited an average decrease from 60 to 55 MPa due to the presence of CB, which is typically known to reduce the mechanical properties with high porosity. In XRD results, the muscovite phase is represented by a few of peaks with significant intensities, while the rest peaks are of undetermined phase. The strongest peak at a 26° of 2θ angle, suggesting the presence of potassium and aluminium in the form of silicate minerals.
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来源期刊
AIMS Materials Science
AIMS Materials Science MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
3.60
自引率
0.00%
发文量
33
审稿时长
4 weeks
期刊介绍: AIMS Materials Science welcomes, but not limited to, the papers from the following topics: · Biological materials · Ceramics · Composite materials · Magnetic materials · Medical implant materials · New properties of materials · Nanoscience and nanotechnology · Polymers · Thin films.
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