2014年JCOMM海水盐度测量中试比对项目综述

Q4 Engineering Ocean and Polar Research Pub Date : 2016-09-30 DOI:10.4217/OPR.2016.38.3.247
Jung-Han Lee, Eun-soo Kim, Yong-Kuk Lee
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引用次数: 0

摘要

2014年,JCOMM (WMO/IOC海洋学和海洋气象学联合技术委员会)首次开展了海水盐度测量相互比较项目,有来自16个国家的25个实验室参与。样品A和样品B的盐度值分别为30 ~ 35和20 ~ 25,具有足够的均匀性和稳定性。参与者在自己的实验室中测量了至少3次盐度,并报告了结果。对结果进行统计处理,以评估实验室之间的差异。25个实验室中有20个使用实验室盐度计,该组的统计数据被标记为属于α组;而25个实验室中有5个使用手持式测量仪器,该组的统计数据被表示为属于β组。α组实验室间差异所描述的偏差在±0.001以内,扩展不确定度(k = 2)在0.002附近。在α组中,韩国海洋科学技术研究院(KIOST)的偏倚和不确定度分别为0.000和0.002。由于仪器精度的限制,β组的偏倚大于α组。β组中3个实验室的偏差超过了相应仪器的精度规范。考虑到标准海水(SSW)的不确定度在0.001 ~ 0.002之间,对比结果表明,25个实验室中有16个实验室的测量质量较高,彼此之间基本无法区分。
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Summary of 2014 JCOMM Pilot Inter-Comparison Project for Seawater Salinity Measurements
The inter-comparison project for seawater salinity measurements, in which 25 laboratories from 16 countries took part, was conducted by JCOMM (Joint WMO/IOC Technical Commission for Oceanography and Marine Meteorology) for the first time in 2014. Two seawater samples of different salinity values ranging from 30−35 and 20−25 for Sample A and Sample B respectively and which had sufficient homogeneity and stability were distributed to all participants. Participants measured the salinity in their own laboratories at least 3 times and reported the results. Statistical treatments were applied to the results to assess discrepancies among laboratories. 20 out of the 25 laboratories used laboratory salinometers and statistics for this group were denoted as belonging to group α; while 5 out of the 25 laboratories used hand-held measuring instruments and statistics for this group were denoted as belonging to group β. Bias described as discrepancy among laboratories in group α was within ± 0.001 and expanded uncertainty (k = 2) was in the vicinity of 0.002. The bias and the uncertainty of Korea Institute of Ocean Science and Technology (KIOST), in group α, were 0.000 and 0.002, respectively. The biases of group β were greater than group α because of constraints related to instrument accuracy. Biases from 3 laboratories in group β exceed the accuracy specification of the corresponding instruments. Considering that the uncertainty of Standard Seawater (SSW) is of the order 0.001 to 0.002, the inter-comparison results show that 16 laboratories among the 25 laboratories made high quality measurements, largely indistinguishable from one another.
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Ocean and Polar Research
Ocean and Polar Research Engineering-Ocean Engineering
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