含铬羟基磷灰石的合成与表征

S. Sallam, Khairi M. Tohami, A. Sallam, L. I. A. Salem, F. A. Mohamed
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引用次数: 25

摘要

羟基磷灰石(hydroxyapatite, HA)是一种生物相容性材料,与其他种植材料相比,具有优异的骨导电性和与骨无机部分相似的化学成分,是骨科和牙科中用作骨替代材料的生物相容性材料。制备了不同铬浓度的羟基磷灰石(S1)和载Cr羟基磷灰石(S2、S3、S4和S5)。许多用于分析由于替换而发生的变化的技术。采用XRD (x射线衍射)和FTIR(傅里叶变换红外辐射)光谱对制备的HA和载Cr的HA进行了分析。采用差热分析(DTA)研究了热处理对试样组织变化的影响。结果表明,所有样品具有相同的晶体结构。随着铬离子浓度的增加,样品的结晶度降低。
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Synthesis and characterization of hydroxyapatite contain chromium
Hydroxy apatite (HA) is a biocompatible material used as bone-substitute materials in both orthopedics and dentistry due to its excellent osteo-conductive and chemical composition similar to that of the inorganic part of bone in comparison with other implant materials . HA (S1) and Cr loaded hydroxy apatite (S2, S3, S4 and S5) of different chromium concentrations have been prepared. many techniques used to analyze the changes occurred due to the substitution. The XRD (X-ray diffraction) and FTIR (Fourier transform infrared radiation )spectroscopy were used as analytical techniques for the prepared HA and Cr loaded HA. The effect of the heat treatment on structural change of the samples was examined by DTA. It was found that all the samples have the same crystalline structure. The crystallinity of the samples decreased as the chromium ions concentration increase.
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