{"title":"Camphorapyrazine片段微波辅助合成Carba-和Triazolehemiporphyrazines及表征","authors":"A. S. Kuznetsova, M. Islyaikin, T. Torres","doi":"10.6060/mhc210336k","DOIUrl":null,"url":null,"abstract":"A series of new hemiporphyrazines bearing camphorapyrazine fragments were synthesized using microwave assisted solvent-free protocol by interaction of m-phenylenediamine, 1(H)- or 1-dodecyl-3,5-diamino-1,2,4-triazole with racemic mixture, R-(+)- or S-(-)-camphoradicyanopyrazines. The obtained macroheterocycles were characterized by mass spectrometry, UV-Vis, IR, 1 H and 13 C NMR spectroscopy and elemental analysis data.","PeriodicalId":18090,"journal":{"name":"Macroheterocycles","volume":null,"pages":null},"PeriodicalIF":1.0000,"publicationDate":"2021-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Microwave-Assisted Synthesis and Characterization of Carba- and Triazolehemiporphyrazines with Camphorapyrazine Fragments\",\"authors\":\"A. S. Kuznetsova, M. Islyaikin, T. Torres\",\"doi\":\"10.6060/mhc210336k\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A series of new hemiporphyrazines bearing camphorapyrazine fragments were synthesized using microwave assisted solvent-free protocol by interaction of m-phenylenediamine, 1(H)- or 1-dodecyl-3,5-diamino-1,2,4-triazole with racemic mixture, R-(+)- or S-(-)-camphoradicyanopyrazines. The obtained macroheterocycles were characterized by mass spectrometry, UV-Vis, IR, 1 H and 13 C NMR spectroscopy and elemental analysis data.\",\"PeriodicalId\":18090,\"journal\":{\"name\":\"Macroheterocycles\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":1.0000,\"publicationDate\":\"2021-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Macroheterocycles\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://doi.org/10.6060/mhc210336k\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Macroheterocycles","FirstCategoryId":"92","ListUrlMain":"https://doi.org/10.6060/mhc210336k","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
Microwave-Assisted Synthesis and Characterization of Carba- and Triazolehemiporphyrazines with Camphorapyrazine Fragments
A series of new hemiporphyrazines bearing camphorapyrazine fragments were synthesized using microwave assisted solvent-free protocol by interaction of m-phenylenediamine, 1(H)- or 1-dodecyl-3,5-diamino-1,2,4-triazole with racemic mixture, R-(+)- or S-(-)-camphoradicyanopyrazines. The obtained macroheterocycles were characterized by mass spectrometry, UV-Vis, IR, 1 H and 13 C NMR spectroscopy and elemental analysis data.
期刊介绍：
The journal is a forum for the specialists investigating macroheterocyclic compounds. It publishes original experimental and theoretical works (full papers and short communications) and reviews on synthesis, structural characterization, physical and coordination chemistry as well as practical application of macroheterocycles.
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