{"title":"磷酸二肼的Vilsmeier-Haack反应:4-{[(二甲基)氮杂肼氯铵]甲基}氨基-2,3-二氢-3-氧-4 H - 1,2,4,3 -三氮杂磷孔的合成","authors":"T. Ali, S. M. Abdel‐kariem","doi":"10.5923/J.IJMC.20120205.02","DOIUrl":null,"url":null,"abstract":"A simp le method for the synthesis of 4-{((dimethyl)azanylidenonium ch loride) methyl}amino-2,3-dihydro- 3-o xo -4H-1,2,4,3-t riazaphosphole (2) is described. Treat ment of phosphonic dihydrazide (1 ) with Vilsmeier-Haack reagent led direct ly to the title co mpound in high yield.","PeriodicalId":14124,"journal":{"name":"International Journal of Mobile Communications","volume":"2 1","pages":"192-196"},"PeriodicalIF":0.7000,"publicationDate":"2013-01-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Vilsmeier-Haack Reaction of Phosphonic Dihydrazide: Synthesis of 4- {[(Dimethyl)azanylidenonium Chloride] Methyl} Amino-2,3-Dihydro-3-Oxo-4 H -1,2,4, 3-Triazaphosphole\",\"authors\":\"T. Ali, S. M. Abdel‐kariem\",\"doi\":\"10.5923/J.IJMC.20120205.02\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A simp le method for the synthesis of 4-{((dimethyl)azanylidenonium ch loride) methyl}amino-2,3-dihydro- 3-o xo -4H-1,2,4,3-t riazaphosphole (2) is described. Treat ment of phosphonic dihydrazide (1 ) with Vilsmeier-Haack reagent led direct ly to the title co mpound in high yield.\",\"PeriodicalId\":14124,\"journal\":{\"name\":\"International Journal of Mobile Communications\",\"volume\":\"2 1\",\"pages\":\"192-196\"},\"PeriodicalIF\":0.7000,\"publicationDate\":\"2013-01-07\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Mobile Communications\",\"FirstCategoryId\":\"91\",\"ListUrlMain\":\"https://doi.org/10.5923/J.IJMC.20120205.02\",\"RegionNum\":4,\"RegionCategory\":\"管理学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"COMMUNICATION\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Mobile Communications","FirstCategoryId":"91","ListUrlMain":"https://doi.org/10.5923/J.IJMC.20120205.02","RegionNum":4,"RegionCategory":"管理学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"COMMUNICATION","Score":null,"Total":0}
Vilsmeier-Haack Reaction of Phosphonic Dihydrazide: Synthesis of 4- {[(Dimethyl)azanylidenonium Chloride] Methyl} Amino-2,3-Dihydro-3-Oxo-4 H -1,2,4, 3-Triazaphosphole
A simp le method for the synthesis of 4-{((dimethyl)azanylidenonium ch loride) methyl}amino-2,3-dihydro- 3-o xo -4H-1,2,4,3-t riazaphosphole (2) is described. Treat ment of phosphonic dihydrazide (1 ) with Vilsmeier-Haack reagent led direct ly to the title co mpound in high yield.
期刊介绍：
The world of mobile communications is not a trend, but a phenomenon. IJMC, a fully refereed journal, publishes articles that present current practice and theory of mobile communications, mobile technology, and mobile commerce applications. Topics covered include Integrated mobile marketing communications Wireless advertising/CRM Telematics, pervasive computing Incoming/outgoing wireless links Location management Diffusion, security, efficacy, interaction/integration Metric mobile business enterprises PDAs in services delivery M-/u-business models, m-/u-commerce Digital office, groupware, roomware Mobile ad hoc networking, wireless information assurance Nomadic/portable communications Cross-cultural mobile communications Teaching mobile communication applications Mobile/handheld devices in the classroom, tele-learning.
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