台湾重连品种中甾体皂苷的分离与鉴定。

Q4 Immunology and Microbiology Taiwanese Journal of Agricultural Chemistry and Food Science Pub Date : 2010-12-01 DOI:10.6578/TJACFS.2010.034

Deng-Jye Yang, Y. Chang, Shih-Chuan Liu, Mei-Peng Lu, Jau-Tien Lin

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引用次数: 0

摘要

台湾蚤休(Paris formosana Hayata)具有九个类固醇皂苷，其化学结构是利用液-液萃取配合高效能液相层析仪进行分离纯化，再经液相层析质谱仪与核磁共振仪进行结构鉴定得知。此九个类固醇皂苷包括三个furostanol glycosides: 26-O-β-D-glucopyranosyl-22α-methoxyl-(25R)-furost-5-en-3β, 26-diol 3-O-α-L-rhamnopyranosyl-(1→4)-O-α-L-rhamnopyranosyl-(1→4)-O-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranoside, 26-O-β-D-glucopyranosyl-22α-methoxyl-(25R)-furost-5-en-3β, 26-diol 3-O-α-L-rhamnopyranosyl-(1→2)-O-[α-L-arabinofuranosyl-(1→4)]-β-Dglucopyranoside和26-O-β-D-glucopyranosyl-22α-methoxyl-(25R)-furost-5-en-3β, 26-diol 3-O-α-L-rhamnopyranosy-(1→2)-O-[β-D-glucopyranosyl (1→3)]-β-D-glucopyranoside，二个pennogenyl glycosides (spirostanol glycosides): 25 (R)-spirost-5-en-3β, 17-diol 3-O-α-L-rhamnopyranosy-(1→4)-O-α-L-rhamnopyranosyl-(1→4)-O-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranoside和(25R)-spirost-5-en-3β, 17-diol 3-O-α-L-rhamnopyranosyl-(1→2)-[α-L-arabinofuranosyl-(1→4)]-β-D-glucopyranoside以及四个diosgenyl glycosides (spirostanol glycosides): (25R)-spirost-5-en-3β-ol 3-O-α-L-rhamnopyranosyl-(1→4)-O-α-L-rhamnopyranosyl-(1→4)-O-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranoside, 3-O-α-L-rhamnopyranosyl-(1→2)-[β-D-glucopyranoside-(1→3)]-β-D-glucopyranoside, (25R)-spirost-5-en-3β-ol 3-O-α-L-rhamnopyranosyl-(1→2)-[α-L-arabinofuranosyl-(1→4)]-β-D-glucopyranoside (25R)-spirost-5-en-3β-ol和(25R)-spirost-5-en-3β-ol 3-O-α-Lrhamnopyranosyl-(1→2)-O-β-D-glucopyranoside.

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Isolation and identification of steroidal saponins in Taiwanese Rhizoma Paridis cultivar (Paris formosana Hayata).

台灣蚤休(Paris formosana Hayata)具有九個類固醇皂苷，其化學結構是利用液－液萃取配合高效能液相層析儀進行分離純化，再經液相層析質譜儀與核磁共振儀進行結構鑑定得知。此九個類固醇皂苷包括三個furostanol glycosides: 26-O-β-D-glucopyranosyl-22α-methoxyl-(25R)-furost-5-en-3β, 26-diol 3-O-α-L-rhamnopyranosyl-(1→4)-O-α-L-rhamnopyranosyl-(1→4)-O-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranoside, 26-O-β-D-glucopyranosyl-22α-methoxyl-(25R)-furost-5-en-3β, 26-diol 3-O-α-L-rhamnopyranosyl-(1→2)-O-[α-L-arabinofuranosyl-(1→4)]-β-Dglucopyranoside和26-O-β-D-glucopyranosyl-22α-methoxyl-(25R)-furost-5-en-3β, 26-diol 3-O-α-L-rhamnopyranosy-(1→2)-O-[β-D-glucopyranosyl (1→3)]-β-D-glucopyranoside，二個pennogenyl glycosides (spirostanol glycosides): 25 (R)-spirost-5-en-3β, 17-diol 3-O-α-L-rhamnopyranosy-(1→4)-O-α-L-rhamnopyranosyl-(1→4)-O-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranoside和(25R)-spirost-5-en-3β, 17-diol 3-O-α-L-rhamnopyranosyl-(1→2)-[α-L-arabinofuranosyl-(1→4)]-β-D-glucopyranoside以及四個diosgenyl glycosides (spirostanol glycosides): (25R)-spirost-5-en-3β-ol 3-O-α-L-rhamnopyranosyl-(1→4)-O-α-L-rhamnopyranosyl-(1→4)-O-[α-L-rhamnopyranosyl-(1→2)]-β-D-glucopyranoside, 3-O-α-L-rhamnopyranosyl-(1→2)-[β-D-glucopyranoside-(1→3)]-β-D-glucopyranoside, (25R)-spirost-5-en-3β-ol 3-O-α-L-rhamnopyranosyl-(1→2)-[α-L-arabinofuranosyl-(1→4)]-β-D-glucopyranoside (25R)-spirost-5-en-3β-ol和(25R)-spirost-5-en-3β-ol 3-O-α-Lrhamnopyranosyl-(1→2)-O-β-D-glucopyranoside.

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Taiwanese Journal of Agricultural Chemistry and Food Science Immunology and Microbiology-Applied Microbiology and Biotechnology

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