S. Nemoto, K. Sasaki, Syuichi Eto, Isao Saito, H. Sakai, Tetsuo Takahashi, Yasuhide Tonogai, T. Nagayama, S. Hori, Yoshiaki Maekawa, M. Toyoda
{"title":"GC/MS(SIM)对农作物中110个农药进行分析","authors":"S. Nemoto, K. Sasaki, Syuichi Eto, Isao Saito, H. Sakai, Tetsuo Takahashi, Yasuhide Tonogai, T. Nagayama, S. Hori, Yoshiaki Maekawa, M. Toyoda","doi":"10.3358/SHOKUEISHI.41.233","DOIUrl":null,"url":null,"abstract":"農作物からアセトニトリル抽出後, GPC及びカートリッジカラムによるクリーンアップを行い, GC/MS (SIM) 測定する110農薬の一斉分析法を作成した. 6農作物に4又は5分析機関で添加回収試験を行った結果, 各農薬の回収率データ中70~120%の良好な結果を示したデータが全体の70%以上を占めた農薬は77種であった. 各農薬の検出限界値は0.0004~0.08μg/g以下であった.","PeriodicalId":17269,"journal":{"name":"Journal of The Food Hygienic Society of Japan (shokuhin Eiseigaku Zasshi)","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2000-08-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"24","resultStr":"{\"title\":\"GC/MS(SIM)による農作物中110農薬の一斉分析法\",\"authors\":\"S. Nemoto, K. Sasaki, Syuichi Eto, Isao Saito, H. Sakai, Tetsuo Takahashi, Yasuhide Tonogai, T. Nagayama, S. Hori, Yoshiaki Maekawa, M. Toyoda\",\"doi\":\"10.3358/SHOKUEISHI.41.233\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"農作物からアセトニトリル抽出後, GPC及びカートリッジカラムによるクリーンアップを行い, GC/MS (SIM) 測定する110農薬の一斉分析法を作成した. 6農作物に4又は5分析機関で添加回収試験を行った結果, 各農薬の回収率データ中70~120%の良好な結果を示したデータが全体の70%以上を占めた農薬は77種であった. 各農薬の検出限界値は0.0004~0.08μg/g以下であった.\",\"PeriodicalId\":17269,\"journal\":{\"name\":\"Journal of The Food Hygienic Society of Japan (shokuhin Eiseigaku Zasshi)\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2000-08-25\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"24\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of The Food Hygienic Society of Japan (shokuhin Eiseigaku Zasshi)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.3358/SHOKUEISHI.41.233\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of The Food Hygienic Society of Japan (shokuhin Eiseigaku Zasshi)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.3358/SHOKUEISHI.41.233","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}