{"title":"时间-温度冷冻法分析高纯度材料的纯度","authors":"G. Ross, H. D. Dixon","doi":"10.6028/jres.067A.025","DOIUrl":null,"url":null,"abstract":"Visual observation of the freezing and melting of compounds in cells used for the determination of purity has uncovered some heretofore unexpected behavior. This behavior has been correlated with certain difficulties experienced in the measurement of purity, particularly when the sample is very pure. Means for partially reducing these difficulties are proposed and procedures for increasing the accuracy of purity measurements are described.","PeriodicalId":94340,"journal":{"name":"Journal of research of the National Bureau of Standards. Section A, Physics and chemistry","volume":"67 1","pages":"247 - 251"},"PeriodicalIF":0.0000,"publicationDate":"1963-05-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Purity Analysis of Highly Purified Materials by Time-Temperature Cryometry\",\"authors\":\"G. Ross, H. D. Dixon\",\"doi\":\"10.6028/jres.067A.025\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Visual observation of the freezing and melting of compounds in cells used for the determination of purity has uncovered some heretofore unexpected behavior. This behavior has been correlated with certain difficulties experienced in the measurement of purity, particularly when the sample is very pure. Means for partially reducing these difficulties are proposed and procedures for increasing the accuracy of purity measurements are described.\",\"PeriodicalId\":94340,\"journal\":{\"name\":\"Journal of research of the National Bureau of Standards. Section A, Physics and chemistry\",\"volume\":\"67 1\",\"pages\":\"247 - 251\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1963-05-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of research of the National Bureau of Standards. Section A, Physics and chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.6028/jres.067A.025\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of research of the National Bureau of Standards. Section A, Physics and chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.6028/jres.067A.025","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Purity Analysis of Highly Purified Materials by Time-Temperature Cryometry
Visual observation of the freezing and melting of compounds in cells used for the determination of purity has uncovered some heretofore unexpected behavior. This behavior has been correlated with certain difficulties experienced in the measurement of purity, particularly when the sample is very pure. Means for partially reducing these difficulties are proposed and procedures for increasing the accuracy of purity measurements are described.