焦油洗涤器改善椰壳液烟品质

R. M. Sari, S. Gea, B. Wirjosentono, S. Hendrana
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引用次数: 1

摘要

关于液态烟椰壳热解的最具挑战性的问题之一是焦油的存在。对在500℃条件下,采用带焦油洗涤器的热解反应器生产的椰壳液烟的酸度、含水量、密度及含量分析进行了比较。按照ASTM E70标准用pH计测定酸度,按照ASTM E203和ASTM D1744标准用体积卡尔费休滴定法测定含水量,采用AOC 1995测定密度,采用气相色谱-质谱联用(GC-MS)测定二氯甲烷提取物含量。结果表明:液烟的pH范围为pH 2.4 ~ 2.6,含水量为89.970 ~ 94.593%,密度为1.0118 ~ 1.0036 g/mL。羰基含量为5.05 ~ 6.473%,苯酚含量为85.057 ~ 90.024%。结果表明,焦油洗涤器产生的烟液质量优于常规方法产生的烟液质量。
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Quality Improvement of Liquid Smoke of Coconut Shell by Tar Scrubber
: One of the most challenging issues concerning to the pyrolysis of liquid smoke coconut shell is the presence of tar. The acidity, water content, density and content analysis of liquid smoke using coconut shell which produced at 500 o C using pyrolysis reactor equipped with a tar scrubber were compared to liquid smoke produced conventionally. Characterization of acidity of the liquid was measured by pH meter by adhering to ASTM E70, water content by using volumetric Karl Fischer titration method following ASTM E203 and ASTM D1744 method, the density by AOC 1995, and dichloromethane extracts content by gas chromatography-mass spectrometry (GC-MS). The results showed that the pH range of liquid smoke was pH 2.4 to 2.6 with the water content of 89.970 to 94.593%, and the density of 1.0118 to 1.0036 g/mL. The carbonyl and phenol content were 5.05 to 6.473% and 85.057 to 90.024% respectively. From the results can be concluded that the quality of liquid smoke produced by tar scrubber is better than the quality of liquid produced by conventional method.
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