一锅法合成多功能磁铁矿空心纳米球

D. Nguyen, K. Kim
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引用次数: 1

摘要

在没有模板的情况下,合成了具有中空结构的单分散Fe3O4纳米球。乙二醇(EG)溶液中使用廉价无毒的试剂,如FeCl3-6H2O和乙酸铵。空心结构是在许多初级颗粒聚集的基础上形成的,随后是奥斯瓦尔德成熟过程。纳米颗粒具有高饱和磁化强度(81.0 emu/g-1)的铁磁性。
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One-Pot Synthesis of Multifunctional Magnetite Hollow Nanospheres
Monodispersed Fe3O4 nanospheres with hollow interior structures are synthesized without any template. Inexpensive and nontoxic reagents such as FeCl3-6H2O and ammonium acetate are used in the ethylene glycol (EG) solution. The hollow structure is formed based on the aggregation of many primary particles, followed by Oswald ripening process. Those nanoparticles exhibit a ferromagnetic behavior with a high saturation magnetization of 81.0 emu/g-1.
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