当前生产工艺对钴铬和钛亚结构表面粗糙度、氧化层厚度和瓷结合强度的影响

IF 0.2 Q4 DENTISTRY, ORAL SURGERY & MEDICINE Journal of International Clinical Dental Research Organization Pub Date : 2021-12-31 DOI:10.5577/intdentres.2021.vol11.no3.1
Beyza Ünalan Değirmenci, N. Ersoy
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引用次数: 2

摘要

目的:本研究旨在评估采用铸造、铣削和选择性激光烧结技术生产的钴铬(Co-Cr)和钛(Ti)亚结构的氧化层、表面粗糙度和与瓷的结合强度。方法:制作直径为1 cm,厚度为3 mm的圆盘状金属样品180个。根据制造金属基结构的技术(铸造、铣削和sls)和金属基结构的化学成分(co - cr和Ti),将样品分为6组(n=15)。然后用接触式轮廓仪计算样品表面粗糙度平均值(Ra)。进行无损能量色散x射线检查,确保对比显示的层为氧化层,并根据扫描电镜图像计算氧化层的平均厚度。对金属-瓷配合物进行了剪切粘结强度试验,并记录了其破坏类型。采用双向多元方差分析(MANOVA)对不同金属和生产工艺的氧化层厚度、表面粗糙度和剪切结合强度进行比较,采用Tukey 's诚实显著差异(HSD)检验对主效应进行多重比较。结果:双向方差分析显示,在子结构生产中使用的金属和技术对表面粗糙度、氧化层厚度和剪切结合强度有显著影响(p < 0.001)。Ti基团比Co-Cr基团形成更厚的氧化层。在铣削组中观察到低表面粗糙度值。铸态Co-Cr组剪切结合强度最高,为53.8 MPa,铸态Ti组剪切结合强度最低,为32.2 MPa。结论:不存在理想的生产工艺,生产工艺的效果因所用金属而异。如何引用本文:Ünalan Değirmenci B, Ersoy NM。当前生产工艺对钴铬和钛亚结构表面粗糙度、氧化层厚度和瓷结合强度的影响。国际医学杂志,2021;11(3):129-39。https://doi.org/10.5577/intdentres.2021.vol11.no3.1语言修改:本手稿中的英语已由至少两名专业编辑检查,他们都是英语母语者。
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The effects of current production techniques on the surface roughness, oxide layer thickness and porcelain bond strength of cobalt-chromium and titanium substructures
Aim: This study aimed to evaluate the oxide layer, surface roughness, and bond strength with porcelain of cobalt-chromium (Co-Cr) and titanium (Ti) substructures produced using casting, milling and selective laser sintering techniques. Methodology: A total of 180 disc-shaped metal samples with a diameter of 1 cm and a thickness of 3 mm were produced. The samples were divided into six groups (n=15) according to the technique used to produce the metal substructures—casting, milling, and SLS—and the chemical composition of the metal substructure—Co-Cr and Ti. Then roughness averages (Ra) of the sample surfaced were calculated with a contact-type profilometer. Nondestructive energy-dispersive X-ray was performed to ensure that the layer displayed in contrast was the oxide layer, and the average oxide layer thickness was calculated from scanning electron microscope images. Metal-porcelain complexes were subjected to shear bond strength test and failure types were noted. Two-way multivariate analysis of variance (MANOVA) was used to compare oxide layer thickness, surface roughness, and shear bond strength according to the metal and production technique, and Tukey’s honestly significant difference (HSD) test was used for multiple comparisons of the main effects. Results: Two-way MANOVA revealed that the metal and technique used in the substructure production had significant effects on surface roughness, oxide layer thickness and shear bond strength (p < 0.001). Ti groups exhibited thicker oxide layer formation than Co-Cr groups. Low surface roughness values were observed in the milling groups. The highest shear bond strength value (53.8 MPa) was observed in the Co-Cr group produced by casting, while the lowest value (32.2 MPa) was obtained in the Ti group produced by casting. Conclusion: It should be kept in mind that there is no ideal production technique and that the effects of the production technique differ depending on the metal used.   How to cite this article: Ünalan Değirmenci B, Ersoy NM. The effects of current production techniques on the surface roughness, oxide layer thickness and porcelain bond strength of cobalt-chromium and titanium substructures. Int Dent Res 2021;11(3):129-39. https://doi.org/10.5577/intdentres.2021.vol11.no3.1   Linguistic Revision: The English in this manuscript has been checked by at least two professional editors, both native speakers of English.
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