g-C3N4/SrTiO3复合材料的制备、表征及其光催化活性

Kim-Van Nguyen, Hoa Thanh Dong, Thanh Thi Ho, Lieu Thanh Thi Le, Thanh Minh Thi Huynh, Nga N. T. Nguyen
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引用次数: 0

摘要

将g-C3N4和SrTiO3分散在水中,在150℃下水热合成g-C3N4/SrTiO3复合材料,其中SrTiO3以硝酸锶、丙二醇、四氯化钛和氢氧化钠为前驱体,在150℃下水热合成12小时,不添加任何表面活性剂;在520℃下对三聚氰胺进行热解制备g-C3N4。采用x射线衍射(XRD)、红外光谱(IR)、扫描电镜(SEM)、能量色散x射线能谱(EDS)等技术对材料的性能进行了表征。通过在可见光下对亚甲基蓝(MB)的降解来评价材料的光催化活性。与单组分g-C3N4和SrTiO3相比,g-C3N4/SrTiO3复合材料的光催化活性增强。
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Preparation, characterization, and photocatalytic activity of g-C3N4/SrTiO3 composite
The g-C3N4/SrTiO3 composite was hydrothermally synthesized at 150 oC for 12 hours from a dispersed mixture of g-C3N4 and SrTiO3 in water, in which SrTiO3 was hydrothermally synthesized at 150 oC for 12 hours using strontium nitrate, propan-2-ol, titanium tetrachloride and sodium hydroxide as precursors without assistance of any surfactant; and g-C3N4 was prepared by pyrolysis of melamine at 520 oC. The properties of materials were characterized by various techniques such as X-ray diffraction (XRD), infrared spectra (IR), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS). The photocatalytic activity of materials was assessed by degradation of methylene blue (MB) under visible light. The enhancement of photocatalytic activity of the g-C3N4/SrTiO3 composite compared to single components g-C3N4 and SrTiO3 was observed.
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