废红柏果(Artocarpus Champeden)活化H3PO4吸附亚甲基蓝活性炭的合成及表征

C. Bijang, M. Tanasale, Dewi Sri, Tahril Tahril, T. Azis
{"title":"废红柏果(Artocarpus Champeden)活化H3PO4吸附亚甲基蓝活性炭的合成及表征","authors":"C. Bijang, M. Tanasale, Dewi Sri, Tahril Tahril, T. Azis","doi":"10.22487/j24775185.2022.v11.i1.pp56-63","DOIUrl":null,"url":null,"abstract":"Synthesis of activated carbon from cempedak peel waste is carried out to utilize biomass waste. This study aimed to synthesize and characterize activated carbon from cempedak peel waste. The synthesis was carried out by chemical activation using phosphoric acid with a dry impregnation ratio of 1:4 (g sample:g H3PO4). Samples impregnated for 24 hours were then heated at 250℃—and then calcined at 350℃ and 450℃. The XRD and FTIR characterization results indicated that the activated carbon obtained had an amorphous structure and the activated carbon obtained had hydroxyl, carbonyl, and carboxylic groups. Activated carbon with the highest yield was obtained at a temperature of 350, namely 43%. The results of determining the water content of activated carbon obtained are 8.36% at 350 0C and 7.1% at 450 ℃. The value of water content and ash content of activated carbon from the skin of this cempedak fruit has met the Indonesian National Standard (SNI 06-3730-1995). The best-activated carbon yield was at a calcination temperature of 450, with the percentage of adsorption efficiency on methylene blue of 98.88%.","PeriodicalId":17695,"journal":{"name":"Jurnal Akademika Kimia","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2022-02-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Synthesis and Characterization of Activated Carbon from Waste Compedak Fruit (Artocarpus Champeden) Activated H3PO4 as Adsorbent of Methylene Blue\",\"authors\":\"C. Bijang, M. Tanasale, Dewi Sri, Tahril Tahril, T. Azis\",\"doi\":\"10.22487/j24775185.2022.v11.i1.pp56-63\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Synthesis of activated carbon from cempedak peel waste is carried out to utilize biomass waste. This study aimed to synthesize and characterize activated carbon from cempedak peel waste. The synthesis was carried out by chemical activation using phosphoric acid with a dry impregnation ratio of 1:4 (g sample:g H3PO4). Samples impregnated for 24 hours were then heated at 250℃—and then calcined at 350℃ and 450℃. The XRD and FTIR characterization results indicated that the activated carbon obtained had an amorphous structure and the activated carbon obtained had hydroxyl, carbonyl, and carboxylic groups. Activated carbon with the highest yield was obtained at a temperature of 350, namely 43%. The results of determining the water content of activated carbon obtained are 8.36% at 350 0C and 7.1% at 450 ℃. The value of water content and ash content of activated carbon from the skin of this cempedak fruit has met the Indonesian National Standard (SNI 06-3730-1995). The best-activated carbon yield was at a calcination temperature of 450, with the percentage of adsorption efficiency on methylene blue of 98.88%.\",\"PeriodicalId\":17695,\"journal\":{\"name\":\"Jurnal Akademika Kimia\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-02-28\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Jurnal Akademika Kimia\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.22487/j24775185.2022.v11.i1.pp56-63\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Jurnal Akademika Kimia","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.22487/j24775185.2022.v11.i1.pp56-63","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1

摘要

利用生物质废弃物,以松果皮为原料合成活性炭。本研究旨在以松果皮为原料合成活性炭并对其进行表征。用干浸渍比为1:4 (g样品:g H3PO4)的磷酸进行化学活化合成。浸渍24h的试样在250℃下加热,然后在350℃和450℃下煅烧。XRD和FTIR表征结果表明,得到的活性炭具有无定形结构,并且得到的活性炭具有羟基、羰基和羧基。活性炭在350℃下收率最高,为43%。所得活性炭的含水量测定结果在350℃时为8.36%,在450℃时为7.1%。果皮活性炭的含水量和灰分值符合印尼国家标准(SNI 06-3730-1995)。焙烧温度为450℃时,活性炭收率最高,对亚甲基蓝的吸附率为98.88%。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Synthesis and Characterization of Activated Carbon from Waste Compedak Fruit (Artocarpus Champeden) Activated H3PO4 as Adsorbent of Methylene Blue
Synthesis of activated carbon from cempedak peel waste is carried out to utilize biomass waste. This study aimed to synthesize and characterize activated carbon from cempedak peel waste. The synthesis was carried out by chemical activation using phosphoric acid with a dry impregnation ratio of 1:4 (g sample:g H3PO4). Samples impregnated for 24 hours were then heated at 250℃—and then calcined at 350℃ and 450℃. The XRD and FTIR characterization results indicated that the activated carbon obtained had an amorphous structure and the activated carbon obtained had hydroxyl, carbonyl, and carboxylic groups. Activated carbon with the highest yield was obtained at a temperature of 350, namely 43%. The results of determining the water content of activated carbon obtained are 8.36% at 350 0C and 7.1% at 450 ℃. The value of water content and ash content of activated carbon from the skin of this cempedak fruit has met the Indonesian National Standard (SNI 06-3730-1995). The best-activated carbon yield was at a calcination temperature of 450, with the percentage of adsorption efficiency on methylene blue of 98.88%.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
SPF Activity Sunscreen Spray Gel Ethanol Extract of Cinnamon Bark (Cinnamomum burmanii Ness. BI, Syn) Potential Antioxidant Activity in Octyl p - Methoxycinnamate (OPMC) Compound Synthesized by Sonochemical Method Performance of The Composite Electrode of Reduced Graphene Oxide Palm Oil Shell - Zinc Oxide (rGOCKS - ZnO) as a Chemical Oxygen Demand (COD) Sensor by Photoelectrocatalysis Antioxidant Activity Test of Ethanolic Extract of Tempuyung Leaves (Sonchus Arvensis L.) Based on Linoleic - Thiocyanic Method Synthesis of Fluorescent Carbon Dots from Soybean Residuals Using Hydrothermal Method
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1