{"title":"污染石(CsAlSi2O6)的制备及x射线表征","authors":"Sarah Ann Gallagher , Gregory J. McCarthy","doi":"10.1016/0022-1902(81)80382-X","DOIUrl":null,"url":null,"abstract":"<div><p>A systematic study of the preparation of synthetic pollucite (CsAlSi<sub>2</sub>O<sub>6</sub>) by high temperature solid state reaction was performed. Eighteen different combinations of cesium oxide, alumina and silica sources and three firing temperatures were evaluated. The most effective methods of preparing phase-pure pollucite were identified and the chemical compositions of large batches of pollucite prepared by three of these methods were obtained. Reference X-ray powder diffraction data were obtained for the most nearly stoichiometric synthetic pollucite specimen.</p></div>","PeriodicalId":16275,"journal":{"name":"Journal of Inorganic and Nuclear Chemistry","volume":"43 8","pages":"Pages 1773-1777"},"PeriodicalIF":0.0000,"publicationDate":"1981-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0022-1902(81)80382-X","citationCount":"34","resultStr":"{\"title\":\"Preparation and X-ray characterization of pollucite (CsAlSi2O6)\",\"authors\":\"Sarah Ann Gallagher , Gregory J. McCarthy\",\"doi\":\"10.1016/0022-1902(81)80382-X\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>A systematic study of the preparation of synthetic pollucite (CsAlSi<sub>2</sub>O<sub>6</sub>) by high temperature solid state reaction was performed. Eighteen different combinations of cesium oxide, alumina and silica sources and three firing temperatures were evaluated. The most effective methods of preparing phase-pure pollucite were identified and the chemical compositions of large batches of pollucite prepared by three of these methods were obtained. Reference X-ray powder diffraction data were obtained for the most nearly stoichiometric synthetic pollucite specimen.</p></div>\",\"PeriodicalId\":16275,\"journal\":{\"name\":\"Journal of Inorganic and Nuclear Chemistry\",\"volume\":\"43 8\",\"pages\":\"Pages 1773-1777\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1981-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1016/0022-1902(81)80382-X\",\"citationCount\":\"34\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Inorganic and Nuclear Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/002219028180382X\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Inorganic and Nuclear Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/002219028180382X","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Preparation and X-ray characterization of pollucite (CsAlSi2O6)
A systematic study of the preparation of synthetic pollucite (CsAlSi2O6) by high temperature solid state reaction was performed. Eighteen different combinations of cesium oxide, alumina and silica sources and three firing temperatures were evaluated. The most effective methods of preparing phase-pure pollucite were identified and the chemical compositions of large batches of pollucite prepared by three of these methods were obtained. Reference X-ray powder diffraction data were obtained for the most nearly stoichiometric synthetic pollucite specimen.
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