用微波萃取方法合成和碳纳米粒子

Mentik Hulupi, Haryadi, Nabila Sofiyani, Rizka Amalia Nuriana, Retno Indarti, Fauzi Abdilah
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引用次数: 0

摘要

碳纳米点(CNDs)是一种环境友好、无毒且具有光学性质的纳米碳材料。本研究以抗坏血酸为前体,采用微波辅助萃取法合成CNDs。方法。加热4分钟,功率500W,效果最好。合成的CNDs溶液在365 nm紫外光下呈蓝色。紫外可见分光光度计的测量结果显示,其最大波长为341.5 nm,能隙为5.57 eV。傅里叶红外光谱(FTIR)分析结果表明,CNDs在3354.61 cm-1波数处具有-OH(羟基)官能团,在1633.09 cm-1波数处具有C=O官能团。高分辨率透射电镜(HRTEM)表征结果表明,合成的CNDs为球形,粒径范围为2.54 ~ 9.48 nm。
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Sintesis dan Karakterisasi Carbon Nanodots dengan Metode Microwave Assisted Extraction
Carbon nanodots (CNDs) is one of the carbon nanoparticles that are environmentally friendly, non-toxic, and have optical properties. The aim of this study was to synthesize CNDs from ascorbic acid as a precursor using the Microwave Assisted Extraction method. method. Best results are obtained at 4 minutes of heating and 500W of power. The synthesized CNDs solution showed a blue color under 365 nm UV light. The measurement results with UV Vis spectrophotometer showed the maximum wavelength at 341.5 nm with an energy gap of 5.57 eV. The results of the Fourier transform infrared spectroscopy (FTIR) analysis show that CNDs have the -OH (hydroxyl) functional group at a wave number of 3354.61 cm-1 and C=O functional group at a wave number of 1633.09 cm-1. Characterization results using High resolution transmission electron microscopy (HRTEM) showed that CNDs were spherical in shape with a particle size range of 2.54-9.48 nm.
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