聚乙烯亚胺/二硫化钼复合材料去除六价铬的制备与表征

Q2 Materials Science Revista de Chimie Pub Date : 2022-05-02 DOI:10.37358/rc.22.2.8521
W. Lin, M. Tang, Jian Hua Chen, Yang Huang, Q. J. Lin, Y. Huang
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引用次数: 0

摘要

本实验采用聚乙烯亚胺(PEI)对花状二硫化钼表面进行改性,成功合成PEI/MoS2吸附剂,并应用于废水中Cr(VI)的去除。采用透射电镜(TEM)、扫描电镜(SEM)、红外光谱(FTIR)等分析了PEI/MoS2的理化性质。讨论了PEI/MoS2吸附Cr(VI)的影响因素,包括PEI负载、Cr(VI)浓度、pH值等。当溶液温度为25℃,溶液pH为2,PEI/MoS2复合吸附剂浓度为0.1 g/L, Cr(VI)溶液浓度为50 mg/L时,PEI/MoS2-10对Cr(VI)的吸附量为120.7 mg/g。实验表明PEI/MoS2-10对Cr(VI)具有较强的选择性,再生实验表明PEI/MoS2具有较高的可重复使用性。
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Preparation and Characterization of Polyethyleneimine/Moliybdenum Disufide Composite for Hexavalent Chromium Removal from Aqueous Systems
In this experiment, polyethyleneimine (PEI) was used to modify the surface of flower-like molybdenum disulfide, and the PEI/MoS2 adsorbent was successfully synthesized and applied to remove Cr(VI) from wastewater. The physical and chemical property of PEI/MoS2 were analyzed by TEM, SEM and FTIR, etc. The affecting factors of the adsorption of Cr(VI) by PEI/MoS2 were discussed, including the effects of PEI loading, concentration of Cr(VI), pH value, etc. When the solution temperature is 25 oC, the solution pH is 2, the concentration of PEI/MoS2 composites adsorbent and Cr(VI) solution are 0.1 g/L and 50 mg/L, respectively, the adsorption amount of Cr(VI) by PEI/MoS2-10 is 120.7 mg/g. Experiments show that PEI/MoS2-10 has a strong selectivity to Cr(VI), and regeneration experiments show that PEI/MoS2 has a high reusable.
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来源期刊
Revista de Chimie
Revista de Chimie 化学-工程:化工
自引率
0.00%
发文量
54
审稿时长
3-6 weeks
期刊介绍: Revista de Chimie publishes original scientific studies submitted by romanian and foreign researchers and offers worldwide recognition of articles in many countries enabling their review in the publications of other researchers. Published articles are in various fields of research: * Chemistry * Petrochemistry * Chemical engineering * Process equipment * Biotechnology * Environment protection * Marketing & Management * Applications in medicine * Dental medicine * Pharmacy
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