改性多元醇法制备金纳米颗粒的结构与光学性质

L. Việt
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引用次数: 0

摘要

本研究以三水合氯化金(HAuCl4·3H2O)、乙二醇(EG)、聚乙烯吡罗烷酮(PVP)、硼氢化钠(NaBH4)为前体,采用改性多元醇法制备了金纳米颗粒。采用X射线衍射(XRD)、透射电子显微镜(TEM)和紫外-可见-近红外光谱(UV-vis-NIR)对制备的金纳米粒子的结构和性能进行了研究。结果表明,在50 nm范围内成功合成了平均粒径为28.80 nm的金纳米颗粒。结果表明,金纳米粒子的组装过程主要表现在成核、生长和形成过程中。
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Structure and Optical Property of Gold Nanoparticles Synthesized by Modified Polyol Method
In this research, Au nanoparticles were successfully synthesized by modified polyol method with commercial precursors to be gold (III) chloride trihydrate (HAuCl4·3H2O), ethylene glycol (EG), poly(vinylpyrrolidone) (PVP), sodium borohydride (NaBH4). The structure and properties of as-prepared Au nanoparticles have been investigated by X ray diffraction (XRD), transmission electron microscopy (TEM), and UV-vis-NIR spectroscopy. As a result, Au nanoparticles with the average particle size of 28.80 nm were successfully synthesized in the range of about 50 nm. It is evidenced that the assembly of gold nanoparticles was presented in their nucleation, growth, and formation. 
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