紫外可见分光光度法测定蔬菜、土壤和水样中高效氯氟氰菊酯杀虫剂

D. Sahu, Joyce Rai, C. Bhatt, M. Rai, J. Goswami, A. Sahu, T. V. Singh, M. Nirmala, Kalpana Wani, P. Mundeja
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引用次数: 4

摘要

在现代,农药在农业中被广泛使用。高效氯氟氰菊酯(LCT)是一种应用最广泛的农药,主要用于杀灭农田害虫、蝇类、蝇类等,也用于农作物生产。我们开发了一种新的方法来检测LCT杀虫剂,减少其在农业领域的使用。用该方法测定了黄色染料在460 nm处的最大吸光度。并计算出检出限0.001 mg kg-1,定量限0.056 mg kg-1。摩尔吸光度和桑德尔灵敏度分别为1.782 ×107 mol-1 cm-1和9.996 ×10-6µg cm-2。所得黄色染料在25 ml中符合Beer定律限定范围0.5µg ml-1 ~ 16µg ml-1。该方法耗时短,选择性好,操作简便,灵敏度高,成本低。该方法成功地应用于各种土壤、水和蔬菜样品。
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UV-Visible Spectrophotometric Determination of Lambda-Cyhalothrin Insecticide in Vegetables, Soil and Water Samples
In modern age pesticide is used widely in agriculture. Lambda-cyhalothrin (LCT) is one of the most used pesticides which are used as a insecticide to kill pest, tricks, flies etc in agricultural field and it is also used for crop production. We have developed new method to detect LCT insecticide in agriculture field and reduce its uses. In this method we found the maximum absorbance at 460 nm for yellow colour dye. We also calculated limit of detection and limit of quantification 0.001 mg kg-1 and 0.056 mg kg-1 respectively. Molar absorptivity and Sandell’s sensitivity was also calculated and obtained 1.782 ×107 mol-1 cm-1 and 9.996 ×10-6 µg cm-2 respectively. The obtained yellow colour dye obeyed Beer’s law limit range of 0.5 µg ml -1 to 16 µg ml-1 in 25 ml. This method is less time consuming, selective, simple, sensitive and low cost. Present method is successfully applied in various soil, water and vegetable samples.
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