你好,使用部分自动取水装置的加尔奈特烟雾中让卡尔费舍尔在冷凝机中取水

H. Buser
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引用次数: 1

摘要

摘要对现有的卷烟烟气冷凝水含水量测定方法进行了改进,采用自动终点停止卡尔费歇尔滴定仪。因此,整个过程变得更快(滴定时间少于2分钟),更容易(滴定过程中不需要监督)和更好的重现性(测定水量的变异系数为2.5%)。在这三个标准中,自动卡尔费歇尔法优于作为比较方法的气相色谱法。
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The Determination of the Water Content in Cigarette Smoke Condensate Using a Karl Fischer Titrator / Wasserbestimmung im Rauchkondensat nach Karl Fischer mit einer halbautomatischen Apparatur
Abstract The current method of determination of the water content of cigarette smoke condensate was improved by using a Karl Fischer titrator with automatic end-point stop. The overall procedure thus becomes faster (the titration time is less than 2 minutes), easier (no supervision is needed during the titration) and better reproducible (coefficient of variation 2.5 % on the amount of water determined). In these three criterions, the automated Karl Fischer method is superior to a gas-chromatographic procedure having served as a method of comparison.
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Beitrage zur Tabakforschung International/ Contributions to Tobacco Research
Beitrage zur Tabakforschung International/ Contributions to Tobacco Research Agricultural and Biological Sciences-Agronomy and Crop Science
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