{"title":"以蛋白为模板的微波辐射合成ZnO纳米结构","authors":"T. Prakash, R. Jayaprakash, G. Neri, Sanjay Kumar","doi":"10.1155/2013/274894","DOIUrl":null,"url":null,"abstract":"ZnO nanostructures have been successfully prepared by a microwave irradiation method. The role of albumen as a template in addressing the size and morphology of ZnO has been investigated by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetric analysis (TG-DTA), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) techniques. A heterogeneous mixture of Zn(OH)2 and ZnO was obtained in absence of albumen. Pure ZnO nanostructures, consisting of rod- and whisker-like nanoparticles embedded in a sheet matrix, were obtained in the presence of albumen. Optical and photoluminescence (PL) properties of the synthesized samples were also compared. Results obtained indicate that the microwave-assisted method is a promising low temperature, cheap, and fast method for the production of ZnO nanostructures.","PeriodicalId":16507,"journal":{"name":"Journal of Nanoparticles","volume":"61 1","pages":"1-8"},"PeriodicalIF":0.0000,"publicationDate":"2013-02-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"21","resultStr":"{\"title\":\"Synthesis of ZnO Nanostructures by Microwave Irradiation Using Albumen as a Template\",\"authors\":\"T. Prakash, R. Jayaprakash, G. Neri, Sanjay Kumar\",\"doi\":\"10.1155/2013/274894\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"ZnO nanostructures have been successfully prepared by a microwave irradiation method. The role of albumen as a template in addressing the size and morphology of ZnO has been investigated by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetric analysis (TG-DTA), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) techniques. A heterogeneous mixture of Zn(OH)2 and ZnO was obtained in absence of albumen. Pure ZnO nanostructures, consisting of rod- and whisker-like nanoparticles embedded in a sheet matrix, were obtained in the presence of albumen. Optical and photoluminescence (PL) properties of the synthesized samples were also compared. Results obtained indicate that the microwave-assisted method is a promising low temperature, cheap, and fast method for the production of ZnO nanostructures.\",\"PeriodicalId\":16507,\"journal\":{\"name\":\"Journal of Nanoparticles\",\"volume\":\"61 1\",\"pages\":\"1-8\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2013-02-28\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"21\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Nanoparticles\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1155/2013/274894\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Nanoparticles","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1155/2013/274894","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Synthesis of ZnO Nanostructures by Microwave Irradiation Using Albumen as a Template
ZnO nanostructures have been successfully prepared by a microwave irradiation method. The role of albumen as a template in addressing the size and morphology of ZnO has been investigated by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetric analysis (TG-DTA), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) techniques. A heterogeneous mixture of Zn(OH)2 and ZnO was obtained in absence of albumen. Pure ZnO nanostructures, consisting of rod- and whisker-like nanoparticles embedded in a sheet matrix, were obtained in the presence of albumen. Optical and photoluminescence (PL) properties of the synthesized samples were also compared. Results obtained indicate that the microwave-assisted method is a promising low temperature, cheap, and fast method for the production of ZnO nanostructures.