可逆形状记忆合金薄膜作动器的制备及其相变特性

K. Kuribayashi, S. Shimizu, M. Yoshitake, S. Ogawa
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引用次数: 1

摘要

本文介绍了一种可用于微机械的可逆形状记忆合金薄膜作动器的制备工艺和相变特性。将富镍钛镍合金(TiNi)薄膜溅射沉积在岩盐板或铜箔上,经过结晶(800°C-10 min)和形状记忆(400°C-6 h)两步热处理。在室温(R相)和高温(约90℃)(奥氏体相)下的电流加热过程中,显示出可逆的形状记忆效应。采用ICP、DSC、XRD和TEM分析了其金相性能。结果表明,沉淀Ti - 3 - Ni - 4与体Ti一样,在形状记忆效应中起着重要的偏置弹簧作用。得到了形状记忆合金薄膜作动器的制备工艺与相变特性之间的关系,为实现可逆形状记忆合金薄膜作动器提供了理论依据。
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Fabrication and Transformation Characteristics of Reversible Shape Memory Alloy Thin Film Actuators
This paper presents the fabrication process and transformation characteristics of reversible shape memory alloy thin film actuators which are useful for micromachines. Nickel ( Ni ) rich titanium-nickel alloy ( TiNi ) thin films were sputter deposited on rock salt plates or copper foils and heat processed with two steps which were crystallization ( 800 °C-10 min ) and shape memorization ( 400 °C-6 h ). Reversible shape memory effects of the actuators were shown between the room temperature ( R phase ) by natural radiation of heat and high temperature ( about 90 °C) ( Austenite phase ) by electric current heating. Their metallurgical properties were analyzed by ICP, DSC, XRD and TEM. It was found that precipitate, Ti 3 Ni 4 , played an important role as bias springs for the shape memory effect as the same as the bulk TiNi. Consequently, the relationship between the fabrication process and transformation characteristics of the actuators which is useful to realize reversible shape memory alloy thin film actuators for micromachines was obtained.
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