利用开放时间的测量来评估和验证胶凝瓷砖胶粘剂性能稳定性的可能性评估

IF 0.5 4区 工程技术 Q4 CONSTRUCTION & BUILDING TECHNOLOGY Cement Wapno Beton Pub Date : 2022-01-01 DOI:10.32047/cwb.2022.27.4.1
C. Stancu, Dawid Dębski, J. Michalak
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引用次数: 1

摘要

该研究分析了参加实验室间比较计划的27个实验室获得的瓷砖粘合剂在不少于30分钟后的打开时间测量结果。根据ISO 13528的要求对所得结果进行统计分析,并根据EN ISO/IEC 17043中包含的z-score分析标准进行评估。在发送开放时间测量结果的24个实验室中,有22个实验室确认了它们的能力,根据评估标准获得了“满意”的结果。一个实验室得到的结果被归类为“可疑”,另一个实验室得到的结果被归类为“不满意”。从参与实验室间比较的实验室的角度来看,所获得的结果应被评估为满意,从而实验室确认其能力。然而,应该注意到开放时间测量结果的广泛分散- 22个实验室的结果被归类为“满意”,获得的结果从0.1 N/mm2到1.0 N/mm2。由粘结强度测定的开启时间测量结果的分散性如此之大,表明该方法准确度太低,不宜用于瓷砖胶粘剂性能稳定性的评估和验证。
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Assessment of the possibility of using the measurement of open time to assess and verify the constancy of performance of cementitious ceramic tile adhesives
The study analyzed the results of open time measurements of ceramic tile adhesives after not less than 30 minutes, obtained by 27 laboratories participating in the interlaboratory comparison program. The obtained results were statistically analyzed following the requirements of ISO 13528 and assessed under the z-score analysis criteria contained in the EN ISO/IEC 17043. 22 out of 24 laboratories that sent the results of the open time measurement confirmed their competencies, obtaining a “satisfactory” result following the evaluation criteria. The result obtained by one laboratory was classified as “questionable”, and another received the result as “unsatisfactory”. From the perspective of laboratories participating in interlaboratory comparisons, the obtained results should be assessed as satisfactory, and thus the laboratories confirm their competence. However, a wide scatter of the results of the open time measurement should be noted – 22 laboratories, the results of which were classified as “satisfactory”, obtained results from 0.1 N/mm2 to 1.0 N/mm2. Such a wide scatter of the results of open time measurements determined by the adhesion strength indicates that this method has too little accuracy, and it should not be used in the assessment and verification of constancy of performance of ceramic tile adhesives.
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来源期刊
Cement Wapno Beton
Cement Wapno Beton CONSTRUCTION & BUILDING TECHNOLOGY-MATERIALS SCIENCE, COMPOSITES
CiteScore
1.30
自引率
28.60%
发文量
0
审稿时长
>12 weeks
期刊介绍: The Publisher of the scientific bimonthly of international circulation, entitled "Cement-Wapno-Beton" ["Cement-Lime-Concrete"], is the Fundacja Cement, Wapno, Beton [Foundation Cement, Lime, Concrete]. The periodical is dedicated to the issues concerning mineral setting materials and concrete. It is concerned with the publication of academic and research works from the field of chemistry and technology of building setting materials and concrete
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