Au/Ag NPS修饰聚苯胺的电化学和生物医学应用

P. Singh, Rajan Patel, K. Kumari, G. K. Mehrotra
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引用次数: 3

摘要

聚苯胺(PANI)具有若干个电子结构,并与掺杂有关。含Fe3O4NPs的聚苯胺复合材料作为具有电、磁特性的聚苯胺,经常被研究。以过硫酸铵为氧化剂和催化剂,以苯胺和盐酸为原料,通过溶液混合法制备聚苯胺。制备了聚苯胺与碳酸钙和金/银纳米粒子的复合材料。采用FTIR、SEM、EDX、电导率等测试技术对聚苯胺纳米复合材料进行了表征。通过SEM、FT-IR和EDX分析证实了CaCO3和Au/Ag NPs在聚苯胺基体中的掺入。CaCO3作为粘结剂,为复合材料提供了强度,这一点可以通过SEM微图清楚地理解。对复合材料的电化学研究表明,用金/银纳米粒子修饰聚苯胺后,其导电性能有所提高。采用纸片扩散法对纳米复合材料对大肠杆菌和金黄色葡萄球菌的抑菌活性进行了测试。
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Au/Ag NPS Decorated PANI For Electrochemical and Biomedical Applications
Polyaniline (PANI) has number of electronic structure and it depends on the doping. PANI composites containing Fe3O4NPs are regularly studied as the PANI having electrical and magnetic features. Herein, PANI was prepared from aniline and HCl by means of solution mixing using ammonium persulphate as oxidizing agent and catalyst. Composites of polyaniline with calcium carbonate and Au/Ag NPs were prepared. Nanocomposites of PANI were characterized using FTIR, SEM, EDX, electrical conductivity measurement techniques. The incorporation of CaCO3 and Au/Ag NPs in polyaniline matrix was confirmed by SEM, FT-IR and EDX results. CaCO3 act as binder and provide strength to the composite which can be clearly understood by SEM microgram. Electrochemical study of composite has been done which showed that on decorating PANI with gold/silver NPs, the conducting properties increases. We successfully tested the antimicrobial activity of nanocomposite via paper disk diffusion method against Escherichia coli and Staphylococcus aureus.
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