室温合成TiO2纳米颗粒对棉织物的持久自洁性能研究。

Himadri Tanaya Mahanta
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摘要

本研究采用Box-Behnken实验设计,采用溶胶-凝胶法在室温下对二氧化钛纳米颗粒进行了合成和优化。采用紫外可见分光光度计对二氧化钛纳米颗粒进行了表征,测定其带隙能为3.31 eV,粒径分析仪(PSA)分析了纳米颗粒的粒径为250 nm,扫描电镜(SEM)分析了纳米颗粒在织物表面的均匀分布。采用垫-干固化法将二氧化钛纳米颗粒应用于棉织物上,以提高棉织物的自洁性能。在初始和20次洗涤后,对染料的降解性能进行了评估,并发现随着纳米颗粒浓度的增加,K/S值显著降低。对织物的固有性能没有明显的影响。
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Durable Self Cleaning Property on Cotton Fabric by Synthesised TiO2 Nanoparticles at Room Temperature.
In this study, synthesis and optimization of titanium dioxide nanoparticles were carried out at room temperature by sol-gel technique using Box-Behnken design of experiment. Titanium dioxide nanoparticles were characterised using UV-visible spectrophotometer in which the band gap energy was determined as 3.31 eV, particle size analyser (PSA) analysed size of nanoparticles as 250 nm and scanning electron microscope (SEM) showed uniform distribution of nanoparticles on surface of fabric. The titanium dioxide nanoparticles were applied on cotton fabric through pad-dry-cure method to develop self-cleaning property on cotton fabric. The stain degradation property was evaluated initial and after 20 washes and determined significant decrease in K/S value with increase in concentration of nanoparticles. There is no significant effect on inherent properties of fabric to be found.
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