Ihor O. Pokotylo, P. Zadorozhnii, V. Kiselev, O. V. Okhtina, A. V. Kharchenko
{"title":"基于N-(2,2-二氯-1-异硫氰酸乙酯)苯酰胺衍生物的一些新的杂环化合物","authors":"Ihor O. Pokotylo, P. Zadorozhnii, V. Kiselev, O. V. Okhtina, A. V. Kharchenko","doi":"10.2478/achi-2019-0005","DOIUrl":null,"url":null,"abstract":"Abstract Based on the readily available N-(2,2-dichloro-1-(2-(4-methylbenzoyl)-hydrazine-1-carbothioamido)ethyl)benzamide, the corresponding N-(2,2-dichloro-1-((5-(p-tolyl)-1,3,4-oxadiazol-2-yl)amino)ethyl)benzamide and 5-(p-tolyl)-1,3,4-thiadiazol-2-amine were obtained. The products were received in acceptable yields and were isolated from the reaction mixture without any particular difficulty. The structure of the compounds obtained was confirmed by 1H, 13C NMR spectroscopy and mass spectrometry data.","PeriodicalId":6958,"journal":{"name":"Acta Chemica Iasi","volume":"23 1","pages":"65 - 72"},"PeriodicalIF":0.4000,"publicationDate":"2019-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Some New Heterocyclisations Based on N-(2,2-dichloro-1-isothiocyanatoethyl)benzamide Derivatives\",\"authors\":\"Ihor O. Pokotylo, P. Zadorozhnii, V. Kiselev, O. V. Okhtina, A. V. Kharchenko\",\"doi\":\"10.2478/achi-2019-0005\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Abstract Based on the readily available N-(2,2-dichloro-1-(2-(4-methylbenzoyl)-hydrazine-1-carbothioamido)ethyl)benzamide, the corresponding N-(2,2-dichloro-1-((5-(p-tolyl)-1,3,4-oxadiazol-2-yl)amino)ethyl)benzamide and 5-(p-tolyl)-1,3,4-thiadiazol-2-amine were obtained. The products were received in acceptable yields and were isolated from the reaction mixture without any particular difficulty. The structure of the compounds obtained was confirmed by 1H, 13C NMR spectroscopy and mass spectrometry data.\",\"PeriodicalId\":6958,\"journal\":{\"name\":\"Acta Chemica Iasi\",\"volume\":\"23 1\",\"pages\":\"65 - 72\"},\"PeriodicalIF\":0.4000,\"publicationDate\":\"2019-06-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Acta Chemica Iasi\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2478/achi-2019-0005\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta Chemica Iasi","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2478/achi-2019-0005","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
Some New Heterocyclisations Based on N-(2,2-dichloro-1-isothiocyanatoethyl)benzamide Derivatives
Abstract Based on the readily available N-(2,2-dichloro-1-(2-(4-methylbenzoyl)-hydrazine-1-carbothioamido)ethyl)benzamide, the corresponding N-(2,2-dichloro-1-((5-(p-tolyl)-1,3,4-oxadiazol-2-yl)amino)ethyl)benzamide and 5-(p-tolyl)-1,3,4-thiadiazol-2-amine were obtained. The products were received in acceptable yields and were isolated from the reaction mixture without any particular difficulty. The structure of the compounds obtained was confirmed by 1H, 13C NMR spectroscopy and mass spectrometry data.