{"title":"(S)-1-(4-氯苯甲酰基)-3-(1-羟基-3-苯丙基-2-基)硫脲的晶体结构","authors":"Junke Wang, Zhijin Lu, J. Bai, Yi Pan","doi":"10.2116/ANALSCIX.24.X59","DOIUrl":null,"url":null,"abstract":"(S)-1-(4-Chlorobenzoyl)-3-(1-hydroxy-3-phenylpropan-2-yl)thiourea was synthesized and the crystal structure was determined by single-crystal X-ray diffractometry. The carbonyl and thiocarbonyl moieties are pointing in approximately opposite directions, The unit-cell dimensions are a = 7.2302(13)A, b = 7.4899(15)A, c = 16.265(3)A with α = 93.6190(12)°, β = 90.035(2)°, γ = 90.0520(13)° and V = 879.1(3)A.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"12 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"2","resultStr":"{\"title\":\"Crystal Structure of (S)-1-(4-Chlorobenzoyl)-3-(1-hydroxy-3-phenylpropan-2-yl)thiourea\",\"authors\":\"Junke Wang, Zhijin Lu, J. Bai, Yi Pan\",\"doi\":\"10.2116/ANALSCIX.24.X59\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"(S)-1-(4-Chlorobenzoyl)-3-(1-hydroxy-3-phenylpropan-2-yl)thiourea was synthesized and the crystal structure was determined by single-crystal X-ray diffractometry. The carbonyl and thiocarbonyl moieties are pointing in approximately opposite directions, The unit-cell dimensions are a = 7.2302(13)A, b = 7.4899(15)A, c = 16.265(3)A with α = 93.6190(12)°, β = 90.035(2)°, γ = 90.0520(13)° and V = 879.1(3)A.\",\"PeriodicalId\":7796,\"journal\":{\"name\":\"Analytical Sciences: X-ray Structure Analysis Online\",\"volume\":\"12 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2008-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"2\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Analytical Sciences: X-ray Structure Analysis Online\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2116/ANALSCIX.24.X59\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Analytical Sciences: X-ray Structure Analysis Online","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2116/ANALSCIX.24.X59","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 2
摘要
合成了(S)-1-(4-氯苯甲酰基)-3-(1-羟基-3-苯丙基-2-基)硫脲，并用单晶x射线衍射法测定了其晶体结构。羰基和硫羰基部分大致指向相反的方向，单位胞尺寸为a = 7.2302(13) a, b = 7.4899(15) a, c = 16.265(3) a， α = 93.6190(12)°，β = 90.035(2)°，γ = 90.0520(13)°，V = 879.1(3) a。
Crystal Structure of (S)-1-(4-Chlorobenzoyl)-3-(1-hydroxy-3-phenylpropan-2-yl)thiourea
(S)-1-(4-Chlorobenzoyl)-3-(1-hydroxy-3-phenylpropan-2-yl)thiourea was synthesized and the crystal structure was determined by single-crystal X-ray diffractometry. The carbonyl and thiocarbonyl moieties are pointing in approximately opposite directions, The unit-cell dimensions are a = 7.2302(13)A, b = 7.4899(15)A, c = 16.265(3)A with α = 93.6190(12)°, β = 90.035(2)°, γ = 90.0520(13)° and V = 879.1(3)A.
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