牙科氧化锆陶瓷的制备及性能研究

Xinjie Liang , Yuexiu Qiu , Shaoxiong Zhou , Xiaoyang Hu , Guangyan Yu , Xuliang Deng
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引用次数: 17

摘要

采用微乳液法和两步烧结法制备了高性能的y2o3稳定的四边形氧化锆多晶陶瓷(Y-TZP)。采用x射线衍射(XRD)、扫描电镜(SEM)和透射电镜(TEM)对反应产物的晶相、形貌和微观结构进行了表征。XRD结果表明,该陶瓷主要由四方氧化锆组成。物理力学性能测试结果表明,Y-TZP全烧结陶瓷的抗弯强度、断裂韧性和密度分别为1150 MPa、5.53 MPa·m1/2和6.08 g/cm3,较适合用于牙体修复。该材料经CAD/CAM系统加工后的牙基冠外形逼真,材料的膨胀系数与釉料的膨胀系数吻合较好。这些结果进一步表明,该产品可作为一种有前景的新型陶瓷材料用于制作牙基冠和牙桥。
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Preparation and properties of dental zirconia ceramics

Y2O3-stabilized tetragonal zirconia polycrystalline (Y-TZP) ceramics with high-performance were prepared for dental application by use of the micro-emulsion and two-step sintering method. The crystal phase, morphology, and microstructure of the reaction products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). XRD results show that the ceramics mainly consist of tetragonal zirconia. Physical and mechanical properties test results show that the bending strength, fracture toughness, and the density of full sintered Y-TZP ceramics are 1150 MPa, 5.53 MPa·m1/2, and 6.08 g/cm3, respectively, which suggest that the material is relatively suitable for dental restoration. The dental base crown machined with this material by CAD/CAM system exhibits a verisimilitude configuration and the material's expansion coefficient well matches that of the glaze. These results further indicate that the product can be used as a promising new ceramic material to fabricate dental base crowns and bridges.

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