G. Batdemberel, Yu Ganchimeg, M. Enkhtuul, O. Enkhtsolmon, G. Munkhsaikhan, Dugerjav Otgonbayar
{"title":"惰性气体流动下纳米Ti3O5晶体的合成与表征","authors":"G. Batdemberel, Yu Ganchimeg, M. Enkhtuul, O. Enkhtsolmon, G. Munkhsaikhan, Dugerjav Otgonbayar","doi":"10.4028/p-ejl789","DOIUrl":null,"url":null,"abstract":"In the research, we show that suboxidic Ti7O13 and rutile TiO2 phases formed in addition to the general Ti3O5 phase when the sintering temperature was set at constant argon gas flow rate. Suboxidic Ti7O13 and rutile TiO2 phases were removed by tuning the flow rate of argon gas at constant sintering temperature. At the 1300°C temperature, the smallest Ti3O5 nanocrystals with a size of ~9 nm were produced. Flat shaped particles of Ti3O5 crystals were observed in SEM measurements.","PeriodicalId":18861,"journal":{"name":"Nano Hybrids and Composites","volume":"1 1","pages":"73 - 79"},"PeriodicalIF":0.4000,"publicationDate":"2023-05-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis and Characterization of Nanosized Ti3O5 Crystals under Inert Gas Flow\",\"authors\":\"G. Batdemberel, Yu Ganchimeg, M. Enkhtuul, O. Enkhtsolmon, G. Munkhsaikhan, Dugerjav Otgonbayar\",\"doi\":\"10.4028/p-ejl789\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In the research, we show that suboxidic Ti7O13 and rutile TiO2 phases formed in addition to the general Ti3O5 phase when the sintering temperature was set at constant argon gas flow rate. Suboxidic Ti7O13 and rutile TiO2 phases were removed by tuning the flow rate of argon gas at constant sintering temperature. At the 1300°C temperature, the smallest Ti3O5 nanocrystals with a size of ~9 nm were produced. Flat shaped particles of Ti3O5 crystals were observed in SEM measurements.\",\"PeriodicalId\":18861,\"journal\":{\"name\":\"Nano Hybrids and Composites\",\"volume\":\"1 1\",\"pages\":\"73 - 79\"},\"PeriodicalIF\":0.4000,\"publicationDate\":\"2023-05-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Nano Hybrids and Composites\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.4028/p-ejl789\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"NANOSCIENCE & NANOTECHNOLOGY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Nano Hybrids and Composites","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.4028/p-ejl789","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"NANOSCIENCE & NANOTECHNOLOGY","Score":null,"Total":0}
Synthesis and Characterization of Nanosized Ti3O5 Crystals under Inert Gas Flow
In the research, we show that suboxidic Ti7O13 and rutile TiO2 phases formed in addition to the general Ti3O5 phase when the sintering temperature was set at constant argon gas flow rate. Suboxidic Ti7O13 and rutile TiO2 phases were removed by tuning the flow rate of argon gas at constant sintering temperature. At the 1300°C temperature, the smallest Ti3O5 nanocrystals with a size of ~9 nm were produced. Flat shaped particles of Ti3O5 crystals were observed in SEM measurements.
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