稀有贵金属生产中的分析控制问题

Y. Karpov, V. B. Baranovskaya
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摘要

本文重点讨论了稀有贵金属工业发展中的一个重要问题——分析控制。综述了分析控制作为稀有贵金属生产和产品质量保证的组成部分的发展现状、重要性、问题和前景。介绍了现代分析控制方法,即原子光谱法、质谱法、x射线荧光法和组合法,以及它们的合理应用。报告显示,科学和技术进步与以稀有和贵重金属为基础的材料的命名急剧增加以及对其质量的更高要求是密不可分的。这将需要创建新的和改进现有的分析控制方法,其标准化和计量支持。这项工作应涉及俄罗斯科学院的研究机构、大学、工业研究中心的研究实验室,这些研究中心在苏联解体后在该国幸存下来,并促进植物研究活动。要有效利用国外先进分析实验室的成果,参与国际比较试验。同时,特别注意未解决的问题- -对以稀有和贵重金属为基础的新型产品提出科学合理的要求说明;抽样方法的发展和计量评价;开发高质量的稀有贵金属生产分析控制计量支持改进分析方法;分析方法标准化;认可分析化验室;培养高素质的分析化学家。
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PROBLEMS OF ANALYTICAL CONTROL IN PRODUCTION OF RARE AND PRECIOUS METALS
The article focuses on one of the important issues in rare and precious metals industry development – analytical control. It reviews the current state, importance, problems and prospects for analytical control development as an integral part of the rare and precious metal production and product quality assurance. Modern analytical control methods are described, namely atomic spectral, mass spectral, X-ray fluorescent and combined ones as well as their rational applications. It is shown that scientific and technological progress is inextricably linked with a drastic increase in the nomenclature of materials based on rare and precious metals and higher requirements for their quality. This will require creating new and improving existing analytical control methods, their standardization and metrological support. This work should involve research organizations in theRussianAcademy of Sciences, universities, industry research centers with research laboratories that have survived in the country after theSoviet Union dissolution, as well as promote plant research activities. It is necessary to effectively use the achievements of advanced analytical laboratories abroad, participate in international comparative tests. At the same time, special attention is paid to unsolved problems – scientifically justified statement of requirements for new types of products based on rare and precious metals; development and metrological assessment of sampling methods; development of high-quality metrological support for analytical control of rare and precious metal production; improvement of analytical methods; standardization of analytical methods; accreditation of analytical laboratories; training of highly qualified analytical chemists.
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