水热合成SnO2纳米片及其表征

J. Hassan
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引用次数: 0

摘要

随着人们对纳米材料性能的需求不断增加,纳米材料的合成方法也在不断发展。在120℃的合成温度下,以铁氟纶为衬里的钢为原料,通过简单的一步水热法制备了氧化锡(SnO2)纳米片。采用场发射扫描电子显微镜(FESEM)和x射线衍射仪(XRD)对合成材料进行了表征,揭示了材料的形貌和结构特性。结果表明,制备的SnO2纳米片厚度约为15 nm,具有清晰的片状结构。XRD谱图显示为单相结构,无杂质相。采用稳态光致发光和紫外-可见吸收技术研究了悬浮在乙醇中的纳米片的光学性质。结果表明,在380 nm、445 nm、475 nm和500 nm处有四个峰与近波段发射和缺陷态有关。关键词:SnO2,纳米片,水热,XRD
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Hydrothermal Synthesis and Characterization of SnO2 Nanosheets
Increasing the demand to explore the nanomaterials properties to be used in numerous applications have emerged considerable effort to developing synthesis methods. Herein, Tin oxide (SnO2) nanosheets have been prepared by a facile one step hydrothermal method using Teflon-lined steel at synthesis temperature of 120 C for 12 hours. As synthesis material were characterized by Field emission scanning electron microscopy (FESEM) and x-ray diffraction (XRD) to revealing the morphology and structural properties. As a result, SnO2 nanosheets have been obtained with thickness around 15 nm with a clear sheets morphology. XRD pattern showed one phase structural with absence of impurities phases. Optical properties for nanosheets suspended in ethanol were investigated using steady state photoluminescence and UV-Vis absorption technics. The result showed four peaks centered at 380 nm, 445 nm, 475 nm, and 500 nm related to near band to band emission and defects states. Keywords: SnO2, Nanosheets, hydrothermal, XRD
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