以皂子为天然表面活性剂的氧化锆纳米颗粒的合成与表征,绿色合成方法

Avnish Kumar Arora, Lalit Chauhan, Pankaj Kumar
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引用次数: 0

摘要

以皂果为表面活性剂合成了氧化锆纳米颗粒,并利用XRD、XRD、TEM等分析技术对合成的氧化锆纳米颗粒进行了表征。合成的氧化锆为ZrO2。ZrO2的结构为单斜晶型,磁化率测试表明ZrO2中没有不成对电子。因此ZrO2本质上是抗磁性的。用透射电镜测定了氧化锆的确切尺寸。氧化物的尺寸在13nm - 26nm之间。
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Synthesis and Characterization of Zirconium Oxide Nanoparticles using Sapindus mukorossi (Soapnut) as natural surfactant, A green synthetic approach
Synthesis of zirconium oxide nanoparticles have been carried out in presence of Sapindus mukorossi (Soapnut) as surfactant and characterization of the synthesized nanoparticles have been carried out using analytical techniques as XRD, Magnetic studies and TEM. Synthesized zirconium Oxide was ZrO2. The structure of the ZrO2 was monoclinic Magnetic susceptibility measurements showed that there were no unpaired electrons in ZrO2. Hence ZrO2 is diamagnetic in nature. Exact size of the zirconium oxide were find out using TEM. Size of the oxide was from 13nm – 26nm.
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