{"title":"气相色谱-质谱联用-傅里叶变换-红外(FT-IR)技术筛选感染栎甲醇干瘿提取物","authors":"A. Hussein, G. Mohammed, M. Hadi, I. Hameed","doi":"10.5897/JPP2015.0368","DOIUrl":null,"url":null,"abstract":"The main objective of this study was to determine the phytochemical composition from the dried galls of Quercus infectoria, using methanolic extraction and report the main functional components by using infrared (IR) technique. The phytochemical compound screened by gas chromatography-mass spectrometry (GC-MS) method. Twelve bioactive phytochemical compounds were identified in the methanolic extract of Q. infectoria. The identification of phytochemical compounds is based on the peak area, retention time molecular weight, and molecular formula. GC-MS analysis of Q. infectoria revealed the existence of the Cis-p-mentha -1(7),8-dien-2-ol, 3-Nonynoic acid, Urea, N,N´-bis(2-hydroxyethyl)-, 3-Trifluoroacetoxypentadecane, Pterin -6-carboxylic acid, 2,2-Difluoroheptacosanoic acid, y-Sitosterol, Spirost-8-en-11-one, 3-hydroxy-, (3s,5α,14s,20s,22s,25R)-, Curan,16,17-didehydro-,(20xi.)-, 17.alfa.21s-28,30-Bisnorhopane, Ethyl iso-allocholate, Milbemycin B,6,28-anhydro-15-chloro-25-isopropyl-13-dehydro-5-. The Fourier transform-infrared (FTIR) analysis of Q. infectoria proved the presence of alkenes, aliphatic fluoro compounds, nitro compounds, alkanes, hydrogen bonded alcohols, and phenols. \n \n Key words: Quercus infectoria, Fourier transform-infrared (FT-IR), gas chromatography-mass spectrometry (GC-MS) analysis, phytochemicals.","PeriodicalId":16801,"journal":{"name":"Journal of Pharmacognosy and Phytotherapy","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2016-03-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"58","resultStr":"{\"title\":\"Phytochemical screening of methanolic dried galls extract of Quercus infectoria using gas chromatography-mass spectrometry (GC-MS) and Fourier transform-infrared (FT-IR)\",\"authors\":\"A. Hussein, G. Mohammed, M. Hadi, I. Hameed\",\"doi\":\"10.5897/JPP2015.0368\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The main objective of this study was to determine the phytochemical composition from the dried galls of Quercus infectoria, using methanolic extraction and report the main functional components by using infrared (IR) technique. The phytochemical compound screened by gas chromatography-mass spectrometry (GC-MS) method. Twelve bioactive phytochemical compounds were identified in the methanolic extract of Q. infectoria. The identification of phytochemical compounds is based on the peak area, retention time molecular weight, and molecular formula. GC-MS analysis of Q. infectoria revealed the existence of the Cis-p-mentha -1(7),8-dien-2-ol, 3-Nonynoic acid, Urea, N,N´-bis(2-hydroxyethyl)-, 3-Trifluoroacetoxypentadecane, Pterin -6-carboxylic acid, 2,2-Difluoroheptacosanoic acid, y-Sitosterol, Spirost-8-en-11-one, 3-hydroxy-, (3s,5α,14s,20s,22s,25R)-, Curan,16,17-didehydro-,(20xi.)-, 17.alfa.21s-28,30-Bisnorhopane, Ethyl iso-allocholate, Milbemycin B,6,28-anhydro-15-chloro-25-isopropyl-13-dehydro-5-. The Fourier transform-infrared (FTIR) analysis of Q. infectoria proved the presence of alkenes, aliphatic fluoro compounds, nitro compounds, alkanes, hydrogen bonded alcohols, and phenols. \\n \\n Key words: Quercus infectoria, Fourier transform-infrared (FT-IR), gas chromatography-mass spectrometry (GC-MS) analysis, phytochemicals.\",\"PeriodicalId\":16801,\"journal\":{\"name\":\"Journal of Pharmacognosy and Phytotherapy\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2016-03-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"58\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Pharmacognosy and Phytotherapy\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.5897/JPP2015.0368\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Pharmacognosy and Phytotherapy","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.5897/JPP2015.0368","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Phytochemical screening of methanolic dried galls extract of Quercus infectoria using gas chromatography-mass spectrometry (GC-MS) and Fourier transform-infrared (FT-IR)
The main objective of this study was to determine the phytochemical composition from the dried galls of Quercus infectoria, using methanolic extraction and report the main functional components by using infrared (IR) technique. The phytochemical compound screened by gas chromatography-mass spectrometry (GC-MS) method. Twelve bioactive phytochemical compounds were identified in the methanolic extract of Q. infectoria. The identification of phytochemical compounds is based on the peak area, retention time molecular weight, and molecular formula. GC-MS analysis of Q. infectoria revealed the existence of the Cis-p-mentha -1(7),8-dien-2-ol, 3-Nonynoic acid, Urea, N,N´-bis(2-hydroxyethyl)-, 3-Trifluoroacetoxypentadecane, Pterin -6-carboxylic acid, 2,2-Difluoroheptacosanoic acid, y-Sitosterol, Spirost-8-en-11-one, 3-hydroxy-, (3s,5α,14s,20s,22s,25R)-, Curan,16,17-didehydro-,(20xi.)-, 17.alfa.21s-28,30-Bisnorhopane, Ethyl iso-allocholate, Milbemycin B,6,28-anhydro-15-chloro-25-isopropyl-13-dehydro-5-. The Fourier transform-infrared (FTIR) analysis of Q. infectoria proved the presence of alkenes, aliphatic fluoro compounds, nitro compounds, alkanes, hydrogen bonded alcohols, and phenols.
Key words: Quercus infectoria, Fourier transform-infrared (FT-IR), gas chromatography-mass spectrometry (GC-MS) analysis, phytochemicals.