电沉积制备ni - b - fe2o3复合纳米镀层及其性能

U. Waware, N. Wasekar
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引用次数: 2

摘要

本文研究了以DMAB为硼源电沉积二元Ni-B和三元Ni-B- fe2o3合金镀层。采用FE-SEM、XRD和原子力显微镜(AFM)对镀层的元素组成、相组成和表面形貌进行了表征。采用差示扫描比色法(DSC)研究了涂层的相稳定性。随后,分别利用纳米压痕和动电位极化进行了力学和电化学腐蚀研究。结果表明,在Ni-B合金镀层中添加Fe2O3,镀层硬度比Ni-B镀层提高52%,防腐性能提高3倍。Ni-B- fe2o3涂层是传统化学镀Ni-B合金的一种经济可行的选择。
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Manufacture and Properties of Ni-B-Fe 2 O 3 Composite Nano-coatings by Electrodeposition
Present study deals with electrodeposition of binary Ni-B and ternary Ni-B-Fe2O3 alloy coatings using DMAB as a source of boron. The coatings were characterized for elemental composition, phase composition and surface topography using FE-SEM, XRD and Atomic Force Microscopy (AFM). The phase stability of coatings was studied using differential scanning colorimetry (DSC). Subsequently, the mechanical and electrochemical corrosion studies were carried out using nano indentation and potentiodynamic polarization studies respectively. The results indicate that addition of Fe2O3 in Ni-B alloy coatings results in 52% improvement in hardness and 3 times improvement in corrosion protection efficiency over Ni-B coatings. Ni-B-Fe2O3 coatings can be suitable economical option towards conventional electroless Ni-B alloy.
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