用Mannich反应和他的喀喇昆仑合成基特-褐素

N. T. Berghuis, M. Wahid
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引用次数: 2

摘要

木质素和壳聚糖化合物是自然界中存在的丰富的生物聚合物。然而,这种生物聚合物的使用方面仍然非常小,只成为环境中的废物。利用曼尼希反应合成木质素-壳聚糖可以作为一种替代方法,使木质素废物在未来成为有用的材料。壳聚糖为商品壳聚糖,脱乙酰率为71.57%。使用的表征是FTIR和TGA。在3300 ~ 3500 cm-1波段的FTIR光谱中出现了峰,表明木质素-壳聚糖的合成是成功的。利用热重分析法对木质素-壳聚糖化合物的热降解性能进行了研究。关键词:壳聚糖,木质素,曼尼希反应
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Sintesis kitosan-lignin dengan reaksi Mannich dan karakterisasinya
Lignin and chitosan compounds are abundant biopolymers that occur in nature. However, the use aspect of this biopolymer is still very minimal and only becomes waste in the environment. The synthesis of lignin-chitosan using the Mannich reaction can be an alternative to be able to use this waste to become useful material in the future. The chitosan used was commercial chitosan with% DD (percent deacetylation) of 71.57%. The characterization used is FTIR and TGA. The success of lignin-chitosan synthesis is indicated by the appearance of peaks in the FTIR spectrum at wavenumbers 3300 - 3500 cm-1. TGA analysis is used to determine the thermal degradation properties of lignin-chitosan compounds which are thought to be new biopolymer compounds.   Keywords: Chitosan, Lignin, Mannich Reaction
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