聚酯纤维分散染料5-芳基噻唑衍生物的合成

M. Khalifa, E. Abdel‐Latif, F. Amer, M. Metwally
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引用次数: 12

摘要

通过与各种硫代氨基脲衍生物1的环缩合,制备了一系列5-芳基偶氮-2-(芳基肼基)-2-噻唑啉-4- 1染料3和4。而合成3-氨基- n -(5-芳基偶氮-2-噻唑酰基)-噻唑(2,3-b)吡啶-2-碳酰胺染料8的方法是:2-(n -氯乙酰基)-5-芳基偶氮-噻唑衍生物5与4,6-二甲基-2-巯基烟碱腈反应,然后在含乙醇的乙醇溶液中将得到的硫衍生物7杂环化。将这些染料作为分散染料用于涤纶纤维的染色,并测定了它们的特性和牢度性能。染色纤维表现出优异的洗涤、排汗和升华牢度性能,良好到优异的摩擦牢度和光牢度变化不大。
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Synthesis of Some New 5-Arylazothiazole Derivatives as Disperse Dyes for Dyeing Polyester Fibers
A series of 5-arylazo-2-(arylidenehydrazino)-2-th iazo lin -4-one dyes 3 and 4 was prepared by cyclocondensation of hydrazonoyl bro mides 2 with various thiosemicarbazone derivatives 1. While the synthesis of 3-amino-N-(5-arylazo-2-thiazo lyl)-thieno(2,3-b)pyrid ine-2-carbo xamide dyes 8 was achieved by the reaction of 2-(N-chloroacetyl)-5-ary lazo-thiazo le derivatives 5 with 4,6-dimethyl-2-mercaptonicotinonitrile fo llowed by heterocyclizat ion of the obtained sulfide derivatives 7 in a solution of ethanol containing sodium etho xide. These dyes were applied as disperse dyes for dyeing polyester fibers and their characteristics and fastness properties have been measured. The dyed fibers exh ibit very good to excellent washing, perspiration and sublimat ion fastness properties, with little variation in good to excellent rubbing and light fastness.
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