硬葡聚糖水体系中的低杂质:用全反射x射线荧光分析控制去除过程

S. Boeykens, N. Temprano, C. Vázquez
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引用次数: 7

摘要

摘要:本研究利用全反射x射线荧光(TXRF)测定多糖体系中微量元素,对多糖体系的三种最终纯化方法进行性能研究。TXRF有两个不可缺少的优势来完成这项研究:分析所需的少量样品和避免消化有机物质。研究了仅含杂质的水硬性葡聚糖体系,从稀释溶液到凝胶。在每个浓度范围内选择最有效的纯化工艺。
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LOW IMPURITIES IN SCLEROGLUCAN AQUEOUS SYSTEMS: REMOVAL PROCESSES CONTROL BY TOTAL REFLECTION X-RAY FLUORESCENCE ANALYSIS
ABSTRACT The aim of this work was to use the determination of trace elements by total reflection X-ray fluorescence (TXRF) for the performance study of three final purification methods of polysaccharide systems. TXRF shows two indispensable advantages to accomplish this study: the small quantities of sample required for the analysis and the avoidance of digesting the organic material. Aqueous scleroglucan systems with only impurity traces were studied, from diluted solutions to gels. The most efficient purification process was selected for each range of concentration.
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