利用蒙大拿菱角叶提取物合成纳米银:表征、亚甲基蓝催化降解及抗氧化活性

IF 0.8 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Journal of Nano Research Pub Date : 2022-09-21 DOI:10.4028/p-333bjm
R. Erenler, E. Gecer
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引用次数: 7

摘要

纳米技术是一门发展迅速的研究学科,具有广泛的应用领域。银纳米粒子的合成(sm-AgNPs)是通过还原银离子处理的水提取物蒙大拿牛蒡叶。从黄色到深棕色的颜色变化证实了这些结构。光谱研究揭示了所需的结构。在紫外可见光谱中,在480 nm处观察到最大吸收。在38.14°、44.29°、64.48°和77.38°处的衍射峰(2θ)分别对应111、200、220和311个面,表明纳米结构为面心立方结构。扫描电镜(SEM)和动态光散射(DLS)分析表明,合成的纳米颗粒呈球形,平均粒径为36.42 nm。sm-AgNPs的zeta电位为-35.2 mV,表明纳米颗粒之间存在排斥力和稳定性。傅里叶变换红外光谱仪(FTIR)的峰与酚类、黄酮类、萜类和生物碱相关,表明相应的化合物可能是还原剂。通过对亚甲基蓝的降解考察了sm-AgNPs的光催化效果,在96 h时,sm-AgNPs对染料的降解率约为67%。
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Synthesis of Silver Nanoparticles Using Sideritis montana L. Leaf Extract: Characterization, Catalytic Degradation of Methylene Blue and Antioxidant Activity
Nanotechnology is arising as a fast-developing research discipline with many usages areas. The silver nanoparticles synthesis (sm-AgNPs) is accomplished by reduction of silver ions in treatment with aqueous extract of Sideritis montana L. leaves. The colour change from yellow to dark brown confirmed the structures. The spectroscopic studies revealed the desired structure. In the UV-Vis spectrum, the maximum absorption was observed at 480 nm. The diffraction peaks (2θ) at the degrees of 38.14°, 44.29°, 64.48°, and 77.38° can correspond to 111, 200, 220, and 311 facets that indicates the nanostructure to be a face-centered cubic unit structure. The scanning electron microscope (SEM) and dynamic light scattering (DLS) analyses indicated that the synthesized nanoparticles were spherical with an average particle size of 36.42 nm. The zeta potential of sm-AgNPs was found as -35.2 mV which indicated the repulsion among nanoparticles and their stability. The peaks from Fourier transform infrared spectrometer (FTIR) were associated with the phenols, flavonoids, terpenoids, and alkaloids, indicating that the corresponding compounds might act as reducing agents. The photocatalytic effect of sm-AgNPs was examined by degradation of methylene blue and sm-AgNPs were able to degrade the dye by about 67% at 96 h.
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来源期刊
Journal of Nano Research
Journal of Nano Research 工程技术-材料科学:综合
CiteScore
2.40
自引率
5.90%
发文量
55
审稿时长
4 months
期刊介绍: "Journal of Nano Research" (JNanoR) is a multidisciplinary journal, which publishes high quality scientific and engineering papers on all aspects of research in the area of nanoscience and nanotechnologies and wide practical application of achieved results. "Journal of Nano Research" is one of the largest periodicals in the field of nanoscience and nanotechnologies. All papers are peer-reviewed and edited. Authors retain the right to publish an extended and significantly updated version in another periodical.
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