{"title":"辣椒秸秆活性炭的吸附性能及表征","authors":"H. Dolaş","doi":"10.30931/jetas.1145856","DOIUrl":null,"url":null,"abstract":"This study presented the evaluation of the adsorption of Eriochrome Black T (EBT) on the activated carbon (trH-BS) produced from pepper stalk by activating with 50% phosphoric acid solution (H3PO4) and then by carbonizing at 650 oC for 30 min. in atmosphere of nitrogen (N2) was presented. The isotherm of trH-BS was Type IV, representing micro, meso and macroporous structures. The micropore volume and micropore surface area values of trH-BS were 0.39 cc/g and 1107.294 m2/g, respectively. Also, its meso and macropores had a volume of about 15-17 cc/g and an average surface area of 400 m2/g. The adsorption energy was 18.156 kJ/mol and the BET surface area was 756.257 m2/g. The structure of trH-BS was clarified structurally and morphologically and the formations like nano rod were seen at Scanning Electron Microscopy (SEM) images. By using trH-BS, the adsorption of EBT from the aqueous medium was investigated using 5 different parameters. As a result, it was found that the adsorbents obtained from pepper stalks are suitable for use in EBT adsorption with a ratio of about 50% under suitable conditions.","PeriodicalId":7757,"journal":{"name":"Anadolu University Journal of Science and Technology-A Applied Sciences and Engineering","volume":"61 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2023-08-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"THE ADSORPTION PERFORMANCE and CHARACTERIZATION of THE ACTIVATED CARBON PRODUCED FROM PEPPER STALKS\",\"authors\":\"H. Dolaş\",\"doi\":\"10.30931/jetas.1145856\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"This study presented the evaluation of the adsorption of Eriochrome Black T (EBT) on the activated carbon (trH-BS) produced from pepper stalk by activating with 50% phosphoric acid solution (H3PO4) and then by carbonizing at 650 oC for 30 min. in atmosphere of nitrogen (N2) was presented. The isotherm of trH-BS was Type IV, representing micro, meso and macroporous structures. The micropore volume and micropore surface area values of trH-BS were 0.39 cc/g and 1107.294 m2/g, respectively. Also, its meso and macropores had a volume of about 15-17 cc/g and an average surface area of 400 m2/g. The adsorption energy was 18.156 kJ/mol and the BET surface area was 756.257 m2/g. The structure of trH-BS was clarified structurally and morphologically and the formations like nano rod were seen at Scanning Electron Microscopy (SEM) images. By using trH-BS, the adsorption of EBT from the aqueous medium was investigated using 5 different parameters. As a result, it was found that the adsorbents obtained from pepper stalks are suitable for use in EBT adsorption with a ratio of about 50% under suitable conditions.\",\"PeriodicalId\":7757,\"journal\":{\"name\":\"Anadolu University Journal of Science and Technology-A Applied Sciences and Engineering\",\"volume\":\"61 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-08-24\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Anadolu University Journal of Science and Technology-A Applied Sciences and Engineering\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.30931/jetas.1145856\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Anadolu University Journal of Science and Technology-A Applied Sciences and Engineering","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.30931/jetas.1145856","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
采用50%磷酸(H3PO4)活化后,在氮气(N2)气氛下于650℃下炭化30 min,考察了Eriochrome Black T (EBT)对辣椒秸秆活性炭的吸附性能。trH-BS等温线为IV型,分别代表微孔、介孔和大孔结构。trH-BS的微孔体积和微孔表面积分别为0.39 cc/g和1107.294 m2/g。中孔和大孔的体积约为15 ~ 17 cc/g,平均表面积为400 m2/g。吸附能为18.156 kJ/mol, BET表面积为756.257 m2/g。通过扫描电镜(SEM)对trH-BS的结构和形态进行了澄清,并观察到纳米棒状结构。采用trH-BS,研究了5种不同参数对EBT的吸附效果。实验结果表明,在适宜的条件下,辣椒秸秆吸附剂的吸附比约为50%,可用于EBT吸附。
THE ADSORPTION PERFORMANCE and CHARACTERIZATION of THE ACTIVATED CARBON PRODUCED FROM PEPPER STALKS
This study presented the evaluation of the adsorption of Eriochrome Black T (EBT) on the activated carbon (trH-BS) produced from pepper stalk by activating with 50% phosphoric acid solution (H3PO4) and then by carbonizing at 650 oC for 30 min. in atmosphere of nitrogen (N2) was presented. The isotherm of trH-BS was Type IV, representing micro, meso and macroporous structures. The micropore volume and micropore surface area values of trH-BS were 0.39 cc/g and 1107.294 m2/g, respectively. Also, its meso and macropores had a volume of about 15-17 cc/g and an average surface area of 400 m2/g. The adsorption energy was 18.156 kJ/mol and the BET surface area was 756.257 m2/g. The structure of trH-BS was clarified structurally and morphologically and the formations like nano rod were seen at Scanning Electron Microscopy (SEM) images. By using trH-BS, the adsorption of EBT from the aqueous medium was investigated using 5 different parameters. As a result, it was found that the adsorbents obtained from pepper stalks are suitable for use in EBT adsorption with a ratio of about 50% under suitable conditions.