傅里叶变换红外分光光度计和气相色谱-质谱联用技术研究小茴香的化学成分

Hussein J. Hussein, M. Hadi, I. Hameed
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引用次数: 67

摘要

药用植物是具有生物活性的天然化合物的潜在来源,因此受到世界各国研究者的关注。本研究的目的是测定甲醇提取的种子提取物的化学成分。采用气相色谱-质谱联用(GC-MS)方法筛选植物化合物。从小茴香醇提物中鉴定出56种具有生物活性的植物化学成分。植物化合物的鉴定主要基于峰面积、保留时间、分子量、分子式、质谱片段离子和药理作用。傅里叶变换红外光谱(FTIR)分析结果表明,草芥种子中存在烯烃、脂肪族氟化合物、醇类、醚类、羧酸类、酯类、硝基化合物、烷烃、氢键醇类和酚类化合物。关键词:气相色谱-质谱联用,生物活性化合物,傅里叶变换红外光谱,小茴香
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Study of chemical composition of Foeniculum vulgare using Fourier transform infrared spectrophotometer and gas chromatography - mass spectrometry
Medicinal plants are potential sources of natural compounds with biological activities and therefore attract the attention of researchers worldwide. The objective of this research was to determine the chemical composition of seeds extract from methanol. The phytochemical compound screened by gas chromatography - mass spectrometry (GC-MS) method. Fifty six bioactive phytochemical compounds were identified in the methanolic extract of Foeniculum vulgare. The identification of phytochemical compounds is based on the peak area, retention time molecular weight, molecular formula, MS Fragment- ions and Pharmacological actions. The Fourier transform infrared spectroscopy (FTIR) analysis of F. vulgare seeds proved the presence of alkenes, aliphatic fluoro compounds, alcohols, ethers, carboxlic acids, esters, nitro compounds, alkanes, hydrogen bonded alcohols and phenols. Key words: Gas chromatography - mass spectrometry (GC-MS), bioactive compounds, Fourier transforminfrared spectroscopy (FT-IR), Foeniculum vulgare.
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