水中重金属(As、Cd、Pb、Hg)标准物质的制备研究

Phuong Thao Le Thi, Hang Nguyen Thi, Hong Ha Tran Thi, Chau Nguyen Minh
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引用次数: 0

摘要

标准物质是保证检测结果有效性的重要工具。目前越南标准材料的使用是有限的,因为供应依赖于国外标准材料制造商,成本很高,而国内没有水和食品标准材料生产制造商。本研究旨在为水中重金属Pb、Cd、As和Hg的分析提供一种标准物质的制备方法。标准物质均质,自生产之日起稳定318天。指定值与正常水样中待分析的重金属浓度一致。测量不确定度范围为7.0% ~ 21.7%。这些标准物质可用于实验室内部质量控制。本研究为水中重金属分析标准物质的后续生产时间提供了标准程序,也为进一步用基质和其他分析标准研究标准样品提供了前提。
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Study on the Production of Reference Material of Heavy Metals (As, Cd, Pb, Hg) in Water
Reference materials are an important tool in ensuring the validity of testing results. The use of standard materials in Vietnam is currently limited because the supply depends on foreign standard material manufacturers at a high cost, and there is no domestic manufacturer for water and food reference materials production. This study aims to provide a procedure reference materials production for heavy metals Pb, Cd, As, and Hg analysis in water. The reference materials were homogenized and stable for a period of 318 days from the date of manufacture. With the assigned values consistent with the concentration to be analyzed of the heavy metals in the normal water sample. The measurement uncertainty ranges from 7.0 to 21.7 %. These reference materials can be used for internal quality control for laboratories. The research provides a standard procedure for the following production times for reference materials for heavy metal analysis in water and also a premise for further research on standard samples with matrix and other analytical criteria.
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