玉米芯废还原性氧化石墨烯的合成与表征

D. Perwitasari, Adinata Shafi Wahyudi Suwarno, Muhammad Nauli Rizqi Akbar
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摘要

石墨烯是一种应用广泛的新型碳基纳米材料,具有电学、热学和高导电性等优点。本研究旨在利用改进的Hummer方法从玉米芯废料中合成还原性氧化石墨烯(rGO)并对其进行表征。这是通过去除NaNo3材料来实现的。这种合成使用玉米芯废料制成木炭,粒度为100目,氧化时间为5天。利用傅里叶变换红外光谱(FTIR)和x射线衍射(XRD)对氧化石墨烯进行了结构分析。FTIR测试结果显示,在1568.82 cm-1处有一个带有C=C键的波峰,表明rGO已经形成。XRD测试结果显示,在2θ ~ 24.6635角处存在典型的还原氧化石墨烯材料衍射峰。
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Synthesis and characterization of reduced graphene oxidation from corn cob waste
Graphene is the latest carbon-based nanomaterial with wide applications and has superiority in electrical, thermal, and high conductivity properties. This study aims to synthesize and characterize reduced graphene oxide (rGO) from corncob waste using the modified Hummer method. which was carried out by removing the NaNo3 material. This synthesis used corncob waste that was made into charcoal with a particle size of 100 mesh with an oxidation time of 5 days. Structural analysis of rGO used Fourier Transform Infa Red (FTIR) and X-ray diffraction (XRD) testing. The results of FTIR testing showed a wave peak at 1568.82 cm-1 with C=C bonds which indicated that rGO was formed. The XRD test results showed a diffractogram peak at an angle of 2θ ~ 24.6635 which is typical of rGO materials.
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