这是一种利用六烯光谱学方法在传统市场上循环的汞重金属分析

Vinas Anggraeni
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引用次数: 5

摘要

汞是最危险的化学物质之一,经常被添加到美白霜中。有许多美白霜的制造商或销售商在他们的产品中使用汞,尽管它的使用是被禁止的。本研究对传统市场上的5种美白面霜样品进行了汞的定性和定量分析。用KI试剂进行定性分析,发现5个样品含汞。然后,用原子吸收分光光度计在波长243,7 nm处测定样品中的汞。由验证结果可知,标定曲线得到的回归方程为Y = 0,016779x - 0,04377, LOD和LOQ分别为2,1552µg/L和7,184µg/L。准确度试验表明,回收率在88-97%范围内,精密度试验表明,% RSD值为0.044 -1,57%。五个样本的定量分析结果显示,所有样本的汞含量均在51,576 ppm至3886,776 ppm之间。关键词:美白乳霜;汞;原子吸收分光光度计
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ANALISIS CEMARAN LOGAM BERAT MERKURI DALAM KRIM PEMUTIH WAJAH YANGBEREDAR DIPASAR TRADISIONAL DENGAN METODE SPEKTROFOTOMETRI SERAPANATOM
Mercury is one of the most dangerous chemicals that is often added to whitening cream. There are many manufacturers or sellers of whitening cream who use mercury in their products even though it is use is prohibited. This research conducted a qualitative and quantitative analysis of mercury on five samples of whitening cream in the traditional market. Qualitative analysis was performed using  KI  reagent  and  showed  five  samples  containing  mercury.  Then,  the  determination of mercury in the sample by Atomic Absorption Spectrophotometer at a wavelength of 243,7 nm. From the validation result, the regression equation obtained from the calibration curve is Y = 0,016779x - 0,04377 with LOD and LOQ of 2,1552 µg/L and 7,184 µg/L. The accuracy test is indicated by the percent recovery is in the range 88-97% and the precision test is shown with the % RSD value of 0,044-1,57%. The quantitative analysis results of five samples showed that all samples contained mercury levels range from 51,576 ppm to 3886,776 ppm. Keywords:Whitening cream;Mercury;Atomic Absorption Spectrophotometer.
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