直接汞分析仪(DMA-80)快速测定膳食补充剂中总汞含量的研究与应用

Van Anh Nguyen Thi, Trang Nguyen Thi, Chien Dinh Viet, Giang Tran Hoang, Minh Hien Lu Thi, Chau Nguyen Minh
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摘要

研究了直接汞分析仪(DMA-80)快速准确测定保健品中总汞含量的方法。该方法特异性高,校准曲线相关系数好,R2 > 0.995;检测限(LOD)和定量限(LOQ)分别为1.88µg/kg和6.26µg/kg;相对重复性标准偏差(RSRr)为2.46 ~ 7.34%,加样回收率(R)为85.7 ~ 100%。应用该方法对河内市39份保健品样品中的汞含量进行了评价。初步研究结果表明,市场上13种保健品的初步汞污染范围为5.41 - 450微克/千克。
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Research and application of direct mercury analyzer (DMA-80) quickly determination of total mercury contents in dietary supplements
The Direct Mercury Analyzer (DMA-80) was studied and investigated to quickly and accurately determine the total mercury content in health supplements. The method shows high specificity, and the calibration curve has a good correlation coefficient with R2 greater than 0.995; the limit of detection (LOD) and limit of quantification (LOQ) were 1.88 µg/kg and 6.26 µg/kg, respectively; The relative repeatability standard deviation (RSRr) was in the range of 2.46 - 7.34% and the recovery (R) was in the range of 85.7 - 100%. The method was applied to evaluate the mercury content in 39 health supplement samples taken in Hanoi city. The initial research results indicated preliminary mercury contamination in 13 health supplement products on the market in the range of 5.41 - 450 µg/kg.  
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