热处理对低氮高硼12Cr-3Co钢组织和力学性能的影响

I. Nikitin, A. Fedoseeva, N. Dudova, R. Kaibyshev
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The average sizes of M23C6 carbides and (Ta,Nb)X carbonitrides were about 50 nm and 40 nm, respectively, regardless of tempering temperature. The M6C carbide particles were also observed along the boundaries of prior austenite grains and pockets as well as along the boundaries between δ-ferrite and martensite; their amount was negligible. When tempering temperature increased from 750 to 800°C, the particle density on the boundaries between δ- ferrite/martensite decreased from 3.8 to 0.2 µm-1. A relationship between the lath size (h) and the density of free dislocations (ρ) can be described as h = (5.41/√ρ) - 0.07. Increasing the tempering temperature to 800°C led to a decrease in the hardness up to ∼220 HB, yield stress and ultimate tensile stress up to 520 and 700 MPa, respectively.The effect of heat treatment on the microstructure and mechanical properties of Febal-0.1 wt.%C-12Cr-3Co-2.5W-1Cu-VNbTaBN steel was investigated. After normalization in the range of 1050-1150°C, the martensitic structure was dominant; δ-ferrite content was about 10%. When the temperature of normalizing increased from 1050°C to 1150°C, the average size of prior austenite grains increased from 44 to 68 µm. After tempering at 750, 770 and 800°C, tempered martensitic lath structure with a high dislocation density within martensitic laths contained nanosized M23C6 carbides along the boundaries of prior austenite grains and laths and (Ta,Nb)X carbonitrides randomly distributed in the ferritic matrix. The average sizes of M23C6 carbides and (Ta,Nb)X carbonitrides were about 50 nm and 40 nm, respectively, regardless of tempering temperature. 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引用次数: 0

摘要

研究了热处理对Febal-0.1 wt.%C-12Cr-3Co-2.5W-1Cu-VNbTaBN钢组织和力学性能的影响。1050 ~ 1150℃归一化后,以马氏体组织为主;δ-铁氧体含量约为10%。当正火温度从1050℃升高到1150℃时,奥氏体晶粒的平均尺寸从44µm增加到68µm。在750、770和800℃回火后,回火后的马氏体板条组织中存在高位错密度的纳米级M23C6碳化物,晶粒和板条边界上分布有纳米级M23C6碳化物,铁素体基体中随机分布有(Ta,Nb)X碳氮化物。与回火温度无关,M23C6碳化物和(Ta,Nb)X碳氮化物的平均尺寸分别约为50 nm和40 nm。M6C碳化物颗粒沿奥氏体晶粒和袋状晶界以及δ-铁素体和马氏体晶界分布;它们的数量微不足道。当回火温度从750℃升高到800℃时,δ-铁素体/马氏体界面上的颗粒密度从3.8µm-1降低到0.2µm-1。板条尺寸(h)与自由位错密度(ρ)之间的关系可以描述为h =(5.41/√ρ) - 0.07。将回火温度提高到800℃,硬度降低到~ 220 HB,屈服应力和极限拉伸应力分别降低到520和700 MPa。研究了热处理对Febal-0.1 wt.%C-12Cr-3Co-2.5W-1Cu-VNbTaBN钢组织和力学性能的影响。1050 ~ 1150℃归一化后,以马氏体组织为主;δ-铁氧体含量约为10%。当正火温度从1050℃升高到1150℃时,奥氏体晶粒的平均尺寸从44µm增加到68µm。在750、770和800℃回火后,回火后的马氏体板条组织中存在高位错密度的纳米级M23C6碳化物,晶粒和板条边界上分布有纳米级M23C6碳化物,铁素体基体中随机分布有(Ta,Nb)X碳氮化物。与回火温度无关,M23C6碳化物和(Ta,Nb)X碳氮化物的平均尺寸分别约为50 nm和40 nm。M6C碳化物颗粒沿奥氏体晶粒和袋状晶界以及δ-铁素体和马氏体晶界分布;寡糖……
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Effect of heat treatment on structure and mechanical properties of 12Cr-3Co steel with low N and high B contents
The effect of heat treatment on the microstructure and mechanical properties of Febal-0.1 wt.%C-12Cr-3Co-2.5W-1Cu-VNbTaBN steel was investigated. After normalization in the range of 1050-1150°C, the martensitic structure was dominant; δ-ferrite content was about 10%. When the temperature of normalizing increased from 1050°C to 1150°C, the average size of prior austenite grains increased from 44 to 68 µm. After tempering at 750, 770 and 800°C, tempered martensitic lath structure with a high dislocation density within martensitic laths contained nanosized M23C6 carbides along the boundaries of prior austenite grains and laths and (Ta,Nb)X carbonitrides randomly distributed in the ferritic matrix. The average sizes of M23C6 carbides and (Ta,Nb)X carbonitrides were about 50 nm and 40 nm, respectively, regardless of tempering temperature. The M6C carbide particles were also observed along the boundaries of prior austenite grains and pockets as well as along the boundaries between δ-ferrite and martensite; their amount was negligible. When tempering temperature increased from 750 to 800°C, the particle density on the boundaries between δ- ferrite/martensite decreased from 3.8 to 0.2 µm-1. A relationship between the lath size (h) and the density of free dislocations (ρ) can be described as h = (5.41/√ρ) - 0.07. Increasing the tempering temperature to 800°C led to a decrease in the hardness up to ∼220 HB, yield stress and ultimate tensile stress up to 520 and 700 MPa, respectively.The effect of heat treatment on the microstructure and mechanical properties of Febal-0.1 wt.%C-12Cr-3Co-2.5W-1Cu-VNbTaBN steel was investigated. After normalization in the range of 1050-1150°C, the martensitic structure was dominant; δ-ferrite content was about 10%. When the temperature of normalizing increased from 1050°C to 1150°C, the average size of prior austenite grains increased from 44 to 68 µm. After tempering at 750, 770 and 800°C, tempered martensitic lath structure with a high dislocation density within martensitic laths contained nanosized M23C6 carbides along the boundaries of prior austenite grains and laths and (Ta,Nb)X carbonitrides randomly distributed in the ferritic matrix. The average sizes of M23C6 carbides and (Ta,Nb)X carbonitrides were about 50 nm and 40 nm, respectively, regardless of tempering temperature. The M6C carbide particles were also observed along the boundaries of prior austenite grains and pockets as well as along the boundaries between δ-ferrite and martensite; thei...
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