用于沉积系统的紧凑型旋转基板加热器的设计和构造

Israel Pérez, Tareik Netro, Mario Vazquez, J. Elizalde
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摘要

我们设计并构建了一个紧凑的旋转基板加热器,温度范围从25 $^\circ$C到700 $^\circ$C。该加热器可用于任何需要结晶样品的沉积系统。它的主要功能是在薄膜生长过程中提供原位热处理。温度监测和控制的温度控制器耦合到K型热电偶。设计了一个加热器外壳,以容纳电阻元件,同时允许基板支架自由旋转。旋转不仅对沉积过程中的薄膜均匀性至关重要,而且对消除衬底支架上的温度梯度也至关重要。为了承受氧化和腐蚀环境,仪器由不锈钢制成,不锈钢也可以作为“冷却剂”,利用散热。该仪器在温度稳定的情况下长时间工作性能良好。我们希望这个项目对希望有一个紧凑的旋转加热器满足晶体生长和薄膜均匀性要求的实验室是有用的。
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Design and construction of a compact rotary substrate heater for deposition systems
We have designed and constructed a compact rotary substrate heater for the temperature range from 25 $^\circ$C to 700 $^\circ$C. The heater can be implemented in any deposition system where crystalline samples are needed. Its main function is to provide a heat treatment in situ during film growth. The temperature is monitored and controlled by a temperature controller coupled to a type K thermocouple. A heater case was designed to host a resistive element and at the same time to allow the substrate holder to freely rotate. Rotation is crucial not only for film homogeneity during deposition but also for the elimination of temperature gradients on the substrate holder. To tolerate oxidizing and corrosive environments, the instrument was made of stainless steel which also works as "coolant" taking advantage of heat dissipation. The instrument performs well for long periods of time with stable temperatures. We hope that this project is useful for laboratories wishing to have a compact rotary heater that meets the requirements for crystal growth and film homogeneity.
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