Arpitha Kumari, G. Sanjeev, Boja Poojari, P. Soumya
{"title":"合成杂环有机化合物的结构、光学和热表征","authors":"Arpitha Kumari, G. Sanjeev, Boja Poojari, P. Soumya","doi":"10.9734/ajopacs/2021/v9i430142","DOIUrl":null,"url":null,"abstract":"A heterocyclic organic compound of 3-[(2z)-2-methyl-3-(4-nitrophenyl) prop-2-enoyl]-2H-(1-benzopyran-2-one) (MNB) is synthesized using Claisen-Schmidth condensation reaction. Structural characterization and presence of functional groups are carried out using powder X-ray diffractogram and FTIR spectroscopic studies respectively. Thermogravimetric analysis and differential thermal analysis are carried out to determine the melting property and it shows good thermal stability among organic crystal showing result at 166°C. Second Harmonic Generation efficiency study is carried out using Nd: YAG laser, this revealed that titled compound is good for NLO characterization and applicable in optoelectronics. PL wavelength present in visible region conclude that sample shows fluorescence property.","PeriodicalId":8541,"journal":{"name":"Asian Journal of Physical and Chemical Sciences","volume":"29 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2021-12-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Structural, Optical and Thermal Characterization of Synthesised Heterocyclic Organic Compound\",\"authors\":\"Arpitha Kumari, G. Sanjeev, Boja Poojari, P. Soumya\",\"doi\":\"10.9734/ajopacs/2021/v9i430142\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A heterocyclic organic compound of 3-[(2z)-2-methyl-3-(4-nitrophenyl) prop-2-enoyl]-2H-(1-benzopyran-2-one) (MNB) is synthesized using Claisen-Schmidth condensation reaction. Structural characterization and presence of functional groups are carried out using powder X-ray diffractogram and FTIR spectroscopic studies respectively. Thermogravimetric analysis and differential thermal analysis are carried out to determine the melting property and it shows good thermal stability among organic crystal showing result at 166°C. Second Harmonic Generation efficiency study is carried out using Nd: YAG laser, this revealed that titled compound is good for NLO characterization and applicable in optoelectronics. PL wavelength present in visible region conclude that sample shows fluorescence property.\",\"PeriodicalId\":8541,\"journal\":{\"name\":\"Asian Journal of Physical and Chemical Sciences\",\"volume\":\"29 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2021-12-18\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Asian Journal of Physical and Chemical Sciences\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.9734/ajopacs/2021/v9i430142\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Asian Journal of Physical and Chemical Sciences","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.9734/ajopacs/2021/v9i430142","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Structural, Optical and Thermal Characterization of Synthesised Heterocyclic Organic Compound
A heterocyclic organic compound of 3-[(2z)-2-methyl-3-(4-nitrophenyl) prop-2-enoyl]-2H-(1-benzopyran-2-one) (MNB) is synthesized using Claisen-Schmidth condensation reaction. Structural characterization and presence of functional groups are carried out using powder X-ray diffractogram and FTIR spectroscopic studies respectively. Thermogravimetric analysis and differential thermal analysis are carried out to determine the melting property and it shows good thermal stability among organic crystal showing result at 166°C. Second Harmonic Generation efficiency study is carried out using Nd: YAG laser, this revealed that titled compound is good for NLO characterization and applicable in optoelectronics. PL wavelength present in visible region conclude that sample shows fluorescence property.