伏安法测定食用菌中铂的含量

Diana Amorello, S. Orecchio
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引用次数: 1

摘要

食用菌是一种具有有趣营养价值的食物来源。本研究的主要目的是为蘑菇中铂的定量超痕量分析开发一种一致的方法,这是复杂的,因为它不容易被普通的分析方法定量。本研究是首次建立这些蔬菜中铂含量的分析方法之一。在这项研究中,研究人员调查了来自意大利的28种不同的食用菌样本。采用差分脉冲伏安法(DPV)测定蘑菇中铂的含量。在本研究中,我们采用标准添加法,因为市场上没有认证的含铂族元素的参考蘑菇。铂的定量限为0.03µg kg - 1 d.w.,分析样品中铂的含量在0.03 ~ 73µg kg - 1之间。我们的蘑菇样品的铂含量低于国际机构对其他食品的建议浓度。在未来,优化的方法可用于食品供应的植物和动物基质的分析。
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Quantification of Platinum in Edible Mushrooms Using Voltammetric Techniques
Edible mushrooms are a food source with interesting nutritional values. The chief objective of this research was to develop a consistent method for the quantitative ultra-trace analysis of Pt in mushrooms, which is complex because it cannot be readily quantified by common analytical procedures. This research is one of the first analytical methods to establish Pt amount in these vegetables. In this research, 28 different edible mushroom samples from Italy were investigated. Determination of Pt in mushrooms was completed using Differential Pulse Voltammetry (DPV). In this study, we applied the standard addition method because there are no certified reference mushrooms containing platinum group elements on the market. The platinum quantification limit was 0.03 µg kg−1 d.w. In the analyzed samples, platinum amount was in the range of 0.03–73 µg kg−1. Our mushroom samples had a Pt content lower than the concentrations recommended by international establishments for other foodstuffs. In the future, the optimized method could be used for the analysis of plant and animal matrices intended for food supply.
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