精密温度测量中的校准浴不确定度

IF 0.2 Q4 CHEMISTRY, MULTIDISCIPLINARY Glasnik Hemicara i Tehnologa Bosne i Hercegovine Pub Date : 2019-12-18 DOI:10.35666/ghtbh.2019.53.02
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引用次数: 0

摘要

校准液在世界各地的许多实验室广泛用于比较校准温度计。它们有不同的形状和大小,使用不同的介质(水、酒精、硅油等),但所用介质总是存在一定的不均匀性。在精密温度测量中,校准液的均匀性(均匀性和时间稳定性)至关重要,因为它对总测量不确定度的贡献是最大的。温度梯度可以描述为浴槽工作容积内不同位置的温度变化。暂时的温度稳定性取决于许多因素,如:浴槽温度、控制系统、浴槽结构和浴槽内所用介质的流动,仅举几例。本文研究了圆柱形校准槽的均匀性。均匀性是通过测量槽内的轴向和径向温度梯度来确定的。稳定性是通过观察一定时间内温度读数的变化来检验的。所得结果与制造商规格进行比较,可用于确定温度计校准过程中校准液对总测量不确定度的贡献。
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Calibration bath uncertainty in precision temperature measurements
Calibration baths are widely used in many laboratories worldwide for the calibration of thermometers by comparison. They come in different shapes and sizes and use different media (water, alcohol, silicon oil etc.), but a certain nonuniformity of theused media is always present. During precision temperature measurements, uniformity (homogeneity and temporal stability) of a calibration bath is of the utmost importance since its contribution to total measurement uncertainty is the largest. The temperature gradient can be described as a change of temperature at different positions inside the bath working volume. Temporal temperature stability depends on many factors such as: the bath temperature, control system, bath construction and the flow of the used media inside the bath, just to name a few. In this paper, we investigate uniformity of a cylindrical calibration bath. Homogeneity is determined by measurement of axial and radial temperature gradient inside the bath. Stability is examined by observation of the change in temperature reading during certain period of time. The obtained results are compared with manufacturer specification and can be used for determination of calibration bath contribution to total measurement uncertainty during calibration of thermometers.
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来源期刊
Glasnik Hemicara i Tehnologa Bosne i Hercegovine
Glasnik Hemicara i Tehnologa Bosne i Hercegovine CHEMISTRY, MULTIDISCIPLINARY-
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